期刊首页 优先出版 当期阅读 过刊浏览 作者中心 关于期刊 English

2009年 第3卷 第1期

摘要

关键词

相关研究

回顶部

《化学科学与工程前沿（英文）》 >> 2009年 第3卷 第1期 doi: 10.1007/s11705-009-0108-6

Multiphase surfactant-assisted reaction-separation system in a microchannel reactor

1. Department of Chemical Engineering, Nagoya University, Chikusa, Nagoya 464-8603, Japan; 2. Faculty of Engineering Technology, Al-Balqa Applied University, Amman 11134, Jordan

发布日期： 2009-03-05
HTML17 PDF 2 收藏 0

下一篇 上一篇

摘要

The Lewis acid-catalyzed addition of trimethylsilyl cyanide to -chlorobenzaldehyde in a microchannel reactor was investigated. The microchannel was integrated to promote both reaction and separation of the biphase system. FeF and Cu(triflate) were used as water-stable Lewis acid catalysts. Sodium dodecyl sulfate was incorporated in the organic-aqueous system to enhance the reactivity and to manipulate the multiphase flow inside the microchannel. It was found that the dynamics and the kinetics of the multiphase reaction were affected by the new micellar system. Parallel multiphase flow inside the microchannel was obtained, allowing for continuous and acceptable phase separation. Enhanced selectivity was achieved by operating at lower conversion values.

相关研究