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Progress in membrane distillation crystallization: Process models, crystallization control and innovative

Xiaobin Jiang, Linghan Tuo, Dapeng Lu, Baohong Hou, Wei Chen, Gaohong He

Frontiers of Chemical Science and Engineering 2017, Volume 11, Issue 4,   Pages 647-662 doi: 10.1007/s11705-017-1649-8

Abstract: Membrane distillation crystallization (MDC) is a promising hybrid separation process that has been appliedprogress has been made in MDC technologies including the promotion of nucleation and better control of crystallizationThis review focuses on the development of MDC process models and on crystallization control strategies

Keywords： membrane distillation crystallization     mathematics model     nucleation     separation     hybrid process    

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Membrane Crystallization for Process Intensification and Control: A Review Review

Xiaobin Jiang, Yushan Shao, Lei Sheng, Peiyu Li, Gaohong He

Engineering 2021, Volume 7, Issue 1,   Pages 50-62 doi: 10.1016/j.eng.2020.06.024

Abstract:

Crystallization is a fundamental separation technology used for the production of particulate solidsA novel controlling technology that can simultaneously intensify the overall crystallization processMembrane crystallization (MCr), which has progressed significantly in recent years, is a hybrid technologyThis review illustrates the basic concepts of MCr and its promising applications for crystallizationcontrol and process intensification, including a state-of-the-art review of key MCr-utilized membrane

Keywords： Membrane crystallization     Nucleation     Process control     Process intensification    

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Filtration ability of hollow fiber membrane for production of magnesium ammonium phosphate crystals byreaction crystallization

H. Watamura, H. Marukawa, I. Hirasawa

Frontiers of Chemical Science and Engineering 2013, Volume 7, Issue 1,   Pages 55-59 doi: 10.1007/s11705-013-1312-y

Abstract: between magnesium ammonium phosphate (MAP) crystal properties and the filtration ability of hollow fiber membranePhosphorus recovery process by crystallization has a problem that it produces a large amount of fineSo improvement of the crystallization process by combining with filtration was discussed.MAP crystals were obtained by batch reaction crystallization and the filtration characteristics were

Keywords： membrane separation     crystallization     MAP    

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Effects of a structurally related substance on the crystallization of paracetamol

Ali SALEEMI, I.I. ONYEMELUKWE, Zoltan NAGY

Frontiers of Chemical Science and Engineering 2013, Volume 7, Issue 1,   Pages 79-87 doi: 10.1007/s11705-013-1308-7

Abstract: Paracetamol (PCM) was crystallized from an isopropanol (IPA) solution containing various small amounts of metacetamol as an additive. The effect on the nucleation kinetics was studied by measuring the induction time to nucleation and the metastable zone width using focused beam reflectance measurements (FBRM) and attenuated total reflectance (ATR-UV/Vis) spectroscopy. Both the induction time and the metastable zone width were expressed as functions of the additive concentration. Small amounts of metacetamol (1–4 mol-%) were found to cause significant inhibition to the nucleation by extending both the induction time and the metastable zone width. A progressive change in the morphology of the paracetamol crystals from tabular to columnar habit was observed with increasing metacetamol concentration. The solvent also had a significant effect on the size of the paracetamol crystals as smaller crystals were obtained in IPA than in aqueous solution. The dissolution rate of paracetamol was improved by the incorporation of metacetamol with 4 mol-% having the most effect. A supersaturation control (SSC) approach was implemented for the PCM-IPA system with and without metacetamol in an attempt to control and obtain larger metacetamol-doped paracetamol crystals.

Keywords： acetaminophen     metacetamol     crystallization     metastable zone width     induction time     supersaturation control    

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Interfacial induction and regulation for microscale crystallization process: a critical review

Frontiers of Chemical Science and Engineering 2022, Volume 16, Issue 6,   Pages 838-853 doi: 10.1007/s11705-021-2129-8

Abstract: Microscale crystallization is at the frontier of chemical engineering, material science, and biochemicalstructure and cavities, pore shape and pore size, surface porosity, channels), in various microscale crystallizationfuture research and development directions are outlined to emphasize the importance of interfacial crystallization

Keywords： interfacial crystallization     heterogeneous nucleation     supersaturation     micro/nanostructure     process    

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Importance of emulsions in crystallization—applications for fat crystallization

Sandra PETERSEN, K. CHALEEPA, Joachim ULRICH

Frontiers of Chemical Science and Engineering 2013, Volume 7, Issue 1,   Pages 43-48 doi: 10.1007/s11705-013-1309-6

Abstract: Emulsions and crystallization are two independent research topics which normally do not overlap althoughHere, the importance of emulsions in the field of fat crystallization is described.fractionation and phase change materials, emulsification can be applied as a tool to improve the fat crystallizationemulsification creates new application fields such as solid lipid nanoparticles in the area of fat crystallization

Keywords： emulsion     fat crystallization     phase change material     emulsion fractionation     emulsion solidification    

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Nucleic acid crystallization and X-ray crystallography facilitated by single selenium atom

Wen Zhang,Jack W. Szostak,Zhen Huang

Frontiers of Chemical Science and Engineering 2016, Volume 10, Issue 2,   Pages 196-202 doi: 10.1007/s11705-016-1565-3

Abstract: However, the crystallization and phase determination are the major bottle-neck problems in crystallographystrategies to solve the phase determination problem, but also offer a potential strategy to explore crystallization

Keywords： selenium     DNA     RNA     nucleic acid     crystallization    

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Utilizing melt crystallization fundamentals in the development of a new tabletting technology

Ahmed ABOUZEID,Sandra PETERSEN,Joachim ULRICH

Frontiers of Chemical Science and Engineering 2014, Volume 8, Issue 3,   Pages 346-352 doi: 10.1007/s11705-014-1443-9

Abstract: Increasing production effeciency and lowering costs are some of the many advantages melt crystallizationMelt crystallization is a purification (separation) process.

Keywords： phase separation     melt crystallization     tablets     process optimization    

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The feasibility of coating by cooling crystallization on ibuprofen naked tablets

Fatima Mameri, Ouahiba Koutchoukali, Mohamed Bouhelassa, Anne Hartwig, Leila Nemdili, Joachim Ulrich

Frontiers of Chemical Science and Engineering 2017, Volume 11, Issue 2,   Pages 211-219 doi: 10.1007/s11705-017-1619-1

Abstract: Recently, a new process of coating by cooling crystallization has been developed and applied on bisacodylpastilles obtained by melt crystallization.In this work, we investigated the feasibility of coating by cooling crystallization on ibuprofen “nakedbeen determined experimentally for the coating solution because they are essential factors for any crystallizationThe results show that naked tablet coating by cooling crystallization is feasible and can be applied

Keywords： coating     solution crystallization     ibuprofen tablets     sucrose    

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Preparation and crystallization kinetics of micron-sized Mg(OH)

Xingfu SONG, Kefeng TONG, Shuying SUN, Ze SUN, Jianguo YU

Frontiers of Chemical Science and Engineering 2013, Volume 7, Issue 2,   Pages 130-138 doi: 10.1007/s11705-013-1332-7

Abstract: Furthermore, the crystallization kinetics based on the population balance theory was studied to provide

Keywords： magnesium hydroxide     precipitation     micron-sized     crystallization kinetics    

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Applications of the crystallization process in the pharmaceutical industry

Sohrab ROHANI

Frontiers of Chemical Science and Engineering 2010, Volume 4, Issue 1,   Pages 2-9 doi: 10.1007/s11705-009-0297-z

Abstract: The applications of the crystallization technique in the pharmaceutical industry as a purification andexternal control in the form of feedback and real-time optimal control using cooling and antisolvent crystallizationTwo methods to prepare micron-sized drug particles, namely, micro-crystallization and polymer-coatedResolution of chloromandelic acid derivatives, a racemic compound, is achieved using direct crystallizationand diastereomeric salts crystallization.

Keywords： feedback     morphology     pulmonary     paracetamol     recognition    

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Control of the agglomeration of crystals in the reactive crystallization of 5-(difluoromethoxy)-2-mercapto

Yongli WANG, Shuyuan MA, Xiaodong Lü, Chuang XIE

Frontiers of Chemical Science and Engineering 2012, Volume 6, Issue 4,   Pages 423-431 doi: 10.1007/s11705-012-1211-7

Abstract: The spherical agglomeration of DMB during the reactive crystallization in a batch crystallizer was monitoredWe found that the low feeding rate of acetic acid, high crystallization temperature, low agitation rateIn addition, the crystallization process of DMB was optimized by a new control strategy of supersaturation

Keywords： 5-(difluoromethoxy)-2-mercapto-1H-benzimidazole (DMB)     reactive crystallization     agglomeration     feeding rate     crystallization temperature     agitation rate    

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Modeling of specific structure crystallization coupling with dissolution

Yuanhui JI, Hongliang QIAN, Chang LIU, Xiaohua LU, Xin FENG, Xiaoyan JI,

Frontiers of Chemical Science and Engineering 2010, Volume 4, Issue 1,   Pages 52-56 doi: 10.1007/s11705-009-0301-7

Abstract: In this paper, the research framework for specific structure crystallization modeling has been proposedin which four steps are required in order to investigate the rigorous crystallization modeling by thermodynamicsthe solution, the second is Solid-Liquid equilibrium, the third and fourth are the dissolution and crystallizationcomplex structure formation and microphase transition can be analyzed by combining the dissolution and crystallization

Keywords： structure crystallization     activity coefficient     reference     KCl     dissolution    

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Effects of sucrose crystallization and moisture migration on the structural changes of a coated intermediate

Tiancheng LI, Peng ZHOU, Theodore P. LABUZA

Frontiers of Chemical Science and Engineering 2009, Volume 3, Issue 4,   Pages 346-350 doi: 10.1007/s11705-009-0256-8

Abstract: The purpose of this study was to investigate whether moisture migration and sugar crystallization playmonitored with changes of water activity in different physical domains of samples during storage, while the crystallizationOur results suggested that both moisture loss and sucrose crystallization were mainly responsible forthe crusty intermediate inner layer, and the agglomerated matrix particles were the result of sucrose crystallization

Keywords： inner-layer     agglomerated     IMF     moisture migration     crystallization    

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Title Author Date Type Operation

Progress in membrane distillation crystallization: Process models, crystallization control and innovative

Xiaobin Jiang, Linghan Tuo, Dapeng Lu, Baohong Hou, Wei Chen, Gaohong He

Journal Article

Membrane Crystallization for Process Intensification and Control: A Review

Xiaobin Jiang, Yushan Shao, Lei Sheng, Peiyu Li, Gaohong He

Journal Article

Filtration ability of hollow fiber membrane for production of magnesium ammonium phosphate crystals byreaction crystallization

H. Watamura, H. Marukawa, I. Hirasawa

Journal Article

Jiang Xiaobin: Regulation and Enhancement of Membrane Crystallization Process (2022-4-16)

9 Jun 2022

Conference Videos

Effects of a structurally related substance on the crystallization of paracetamol

Ali SALEEMI, I.I. ONYEMELUKWE, Zoltan NAGY

Journal Article

Interfacial induction and regulation for microscale crystallization process: a critical review

Journal Article

Importance of emulsions in crystallization—applications for fat crystallization

Sandra PETERSEN, K. CHALEEPA, Joachim ULRICH

Journal Article

Nucleic acid crystallization and X-ray crystallography facilitated by single selenium atom

Wen Zhang,Jack W. Szostak,Zhen Huang

Journal Article

Utilizing melt crystallization fundamentals in the development of a new tabletting technology

Ahmed ABOUZEID,Sandra PETERSEN,Joachim ULRICH

Journal Article

The feasibility of coating by cooling crystallization on ibuprofen naked tablets

Fatima Mameri, Ouahiba Koutchoukali, Mohamed Bouhelassa, Anne Hartwig, Leila Nemdili, Joachim Ulrich

Journal Article

Preparation and crystallization kinetics of micron-sized Mg(OH)

Xingfu SONG, Kefeng TONG, Shuying SUN, Ze SUN, Jianguo YU

Journal Article

Applications of the crystallization process in the pharmaceutical industry

Sohrab ROHANI

Journal Article

Control of the agglomeration of crystals in the reactive crystallization of 5-(difluoromethoxy)-2-mercapto

Yongli WANG, Shuyuan MA, Xiaodong Lü, Chuang XIE

Journal Article

Modeling of specific structure crystallization coupling with dissolution

Yuanhui JI, Hongliang QIAN, Chang LIU, Xiaohua LU, Xin FENG, Xiaoyan JI,

Journal Article

Effects of sucrose crystallization and moisture migration on the structural changes of a coated intermediate

Tiancheng LI, Peng ZHOU, Theodore P. LABUZA

Journal Article