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Engineering >> 2019, Volume 5, Issue 3 doi: 10.1016/j.eng.2019.01.013

A Breakthrough in Pressure Generation by a Kawai-Type Multi-Anvil Apparatus with Tungsten Carbide Anvils

a Bayerisches Geoinstitut, University of Bayreuth, Bayreuth 95440, Germany

b State Key Laboratory of Superhard Materials, Jilin University, Changchun 130012, China

c Center for High Pressure Science and Technology Advanced Research, Beijing 100094, China

Received: 2018-07-08 Revised: 2019-01-04 Accepted: 2019-01-28 Available online: 2019-04-26

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Abstract

Expansion of the pressure range of Kawai-type multi-anvil presses (KMAPs) with tungsten carbide (WC) anvils is called for, especially in the field of Earth science. However, no significant progress in pressure generation has been made for 40 years. Our recent studies have expanded the pressure generation of a KMAP with WC anvils to 65 GPa, which is the world record for high-pressure generation in this device and is more than 2.5 times higher than conventional pressure generation. We have also successfully generated pressures of about 50 GPa at high temperatures. This work reviews our recently developed technology for high-pressure generation. High-pressure generation at room temperature and at high temperature was attained by integration of the following techniques: ① a precisely aligned guide-block system, ② a high degree of hardness of the second-stage anvils, ③ tapering of the second-stage anvil faces, ④ a high-pressure cell consisting of materials with a high bulk modulus, and ⑤ high thermal insulation of the furnace. Our high-pressure technology will facilitate investigation of the phase stability and physical properties of materials under the conditions of the upper part of the lower mantle, and will permit the synthesis and characterization of novel materials.

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References

[ 1 ] Ito E. Theory and practice—multianvil cells and high-pressure experimental methods. In: Schubert G, Romanowicz B, Dziewonski A, editors. Treatise on geophysics 2. San Diego: Elsevier; 2007. p. 197–230. link1

[ 2 ] Ovsyannikov SV, Bykov M, Bykova E, Kozlenko DP, Tsirlin AA, Karkin AE, et al. Charge-ordering transition in iron oxide Fe4O5 involving competing dimer and trimer formation. Nat Chem 2016;8(5):501–8. link1

[ 3 ] Keppler H, Frost D. Introduction to minerals under extreme conditions. In: Miletich R, editor. Mineral behavior at extreme conditions. Budapest: Eötvös University Press; 2005. p. 1–30. link1

[ 4 ] Fukao Y, Obayashi M. Subducted slabs stagnant above, penetrating through, and trapped below the 660 km discontinuity. J Geophys Res 2013;118 (11):5920–38. link1

[ 5 ] French SW, Romanowicz B. Broad plumes rooted at the base of the Earth’s mantle beneath major hotspots. Nature 2015;525(7567):95–9. link1

[ 6 ] Wang F, Tange Y, Irifune T, Funakoshi K. P–V–T equation of state of stishovite up to mid-lower mantle conditions. J Geophys Res 2012;117:B06209. link1

[ 7 ] Tange Y, Irifune T, Funakoshi K. Pressure generation to 80 GPa using multianvil apparatus with sintered diamond anvils. High Press Res 2008;28:245–54. link1

[ 8 ] Yamazaki D, Ito E, Yoshino T, Tsujino N, Yoneda A, Guo X, et al. Mbar generation in the Kawai-type multianvil apparatus and its application to compression of (Mg0.92Fe0.08)SiO3 perovskite and stishovite. Phys Earth Planet Inter 2014;228:262–7. link1

[ 9 ] Yamazaki D, Ito E, Yoshino T, Tsujino N, Yoneda A, Gomi H, et al. High-pressure generation in the Kawai-type multianvil apparatus equipped with tungstencarbide anvils and sintered-diamond anvils, and X-ray observation on CaSnO3 and (Mg,Fe)SiO3. Comp Rend Geosci. In press. link1

[10] Ishii T, Shi L, Huang R, Tsujino N, Druzhbin D, Myhill R, et al. Generation of pressures over 40 GPa using Kawai-type multi-anvil press with tungsten carbide anvils. Rev Sci Instrum 2016;87:024501. link1

[11] Ishii T, Yamazaki D, Tsujino N, Xu F, Liu Z, Kawazoe T, et al. Pressure generation to 65 GPa in a Kawai-type multi-anvil apparatus with tungsten carbide anvils. High Press Res 2017;37(4):507–15. link1

[12] Kunimoto T, Irifune T, Tange Y, Wada K. Pressure generation to 50 GPa in Kawai-type multianvil apparatus using newly developed tungsten carbide anvils. High Press Res 2016;36:1–8. link1

[13] Kawai N, Togaya M, Onodera A. A new device for pressure vessels. Proc Jpn Acad 1973;49(8):623–6. link1

[14] Ohtani E, Irifune T, Hibberson WO, Ringwood AE. Modified split-sphere guide block for practical operation of a multiple-anvil apparatus. High Temp High Press 1987;19(5):523–9. link1

[15] Walker D, Carpenter MA, Hitch CM. Some simplifications to multianvil devices for high pressure experiments. Am Miner 1990;75(9–10):1020–8. link1

[16] Osugi J, Shimizu K, Inoue K, Yasunami K. A compact cubic anvil high pressure apparatus. Rev Phys Chem Jpn 1964;34(1):1–6. link1

[17] Katsura T, Funakoshi K, Kubo A, Nishiyama N, Tange Y, Sueda Y, et al. A largevolume high-pressure and high-temperature apparatus for in situ X-ray observation, ‘‘SPEED-Mk.II”. Phys Earth Planet Inter 2004;143–144:497–506. link1

[18] Irifune T. Frontiers in deep earth mineralogy using new large-volume D-DIA and KMA apparatus. Rev High Press Sci Tech 2010;20(2):158–65. link1

[19] Kubo A, Ito E, Katsura T, Shinmei T, Yamada H, Nishikawa O, et al. In situ X-ray observation of iron using Kawai-type apparatus equipped with sintered diamond: absence of b phase up to 44 GPa and 2100 K. Geophys Res Lett 2003;30(3):1126. link1

[20] Irifune T, Adachi Y, Fujino K, Ohtani E, Yoneda A, Sawamoto H. A performance test for WC anvils for multianvil apparatus and phase transformations in some aluminous minerals up to 28 GPa. In: Syono Y, Manghnani MH, editors. Highpressure research: application to earth and planetary sciences. Washington, DC: American Geophysical Union; 1992. p. 43–50. link1

[21] Wada K. Tungsten carbide based hardmetals used for high pressure experiment. Rev High Press Sci Tech 2018;28(1):9–16. link1

[22] Mao HK, Bell PM. Generation of static pressures to 1.5 Mbar. Carnegie Inst Washington 1977;76:644–6. link1

[23] Ito E. The absence of oxide mixture in high-pressure phases of Mg-silicates. Geophys Res Lett 1977;4(2):72–4. link1

[24] Dunn KJ, Bundy FP. Materials and techniques for pressure calibration by resistance-jump transitions up to 500 kilobars. Rev Sci Instrum 1978;49 (3):365–70. link1

[25] Tange Y, Takahashi E, Funakoshi KI. In situ observation of pressure-induced electrical resistance changes in zirconium: pressure calibration points for the large volume press at 8 and 35 GPa. High Press Res 2011;31(3):413–8. link1

[26] Ono S, Kikegawa T. Determination of the phase boundary of the omega to beta transition in Zr using in situ high-pressure and high-temperature X-ray diffraction. J Solid State Chem 2015;225:110–3. link1

[27] Soga N, Anderson OL. High-temperature elastic properties of polycrystalline MgO and Al2O3. J Am Ceram Soc 1966;49:355–9. link1

[28] Liu Z, Nishi M, Ishii T, Fei H, Miyajima N, Ballaran TB, et al. Phase relations in the system MgSiO3–Al2O3 up to 2300 K at lower mantle pressures. J Geophys Res 2017;122(10):7775–88. link1

[29] Ishii T, Sinmyo R, Komabayashi T, Ballaran TB, Kawazoe T, Miyajima N, et al. Synthesis and crystal structure of LiNbO3-type Mg3Al2Si3O12: a possible indicator of shock conditions of meteorites. Am Miner 2017;102(9): 1947–52. link1

[30] Kubo A, Akaogi M. Post-garnet transitions in the system Mg4Si4O12– Mg3Al2Si3O12 up to 28 GPa: phase relations of garnet, ilmenite and perovskite. Phys Earth Planet Inter 2000;121(1–2):85–102. link1

[31] Kubo A. High-pressure experimental study on garnet-perovskite transition in the system MgSiO3–Al2O3 [dissertation]. Tokyo: Gakushuin University; 1999. link1

[32] Tsuchiya T. First-principles prediction of the P–V–T equation of state of gold and the 660-km discontinuity in Earth’s mantle. J Geophys Res 2003;108:2462. link1

[33] Kingery WD, Francl J, Coble RL, Vasilos T. Thermal conductivity: X, data for several pure oxide materials corrected to zero porosity. J Am Ceram Soc 1954;37:107–10. link1

[34] Akaogi M, Ito E, Navrotsky A. Olivine-modified spinel-spinel transitions in the system Mg2SiO4–Fe2SiO4: calorimetric measurements, thermochemical calculation, and geophysical application. J Geophys Res 1989;94:15671–85. link1

[35] Katsura T, Yoneda A, Yamazaki D, Yoshino T, Ito E. Adiabatic temperature profile in the mantle. Phys Earth Planet Inter 2010;183:212–8. link1

[36] Liu Z, Ishii T, Katsura T. Rapid decrease of MgAlO2.5 component in bridgmanite with pressure. Geochem Perspect Lett 2018;5:12–8. link1

[37] Wookey J, Kendall JM, Barruol G. Mid-mantle deformation inferred from seismic anisotropy. Nature 2002;415(6873):777–80. link1

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