《工程(英文)》 >> 2015年 第1卷 第2期 doi: 10.15302/J-ENG-2015040
使用傅里叶变换红外成像进行高通量筛选
SmartState Center for Strategic Approaches to the Generation of Electricity (SAGE), Department of Chemical Engineering, University of South Carolina, Columbia, South Carolina 29208, USA
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摘要
组合库的有效平行筛选是高通量(HT) 多相催化工作流中最具挑战性的难题之一。目前,已有包括各种光学、质谱分析以及气相色谱技术在内的大量方法用于高通量催化剂研究。在这些技术中,快速扫描傅里叶变换红外(FTIR) 成像是最快、最通用的筛选技术。本文介绍了16 通道高通量反应器的新设计,并给出了其准确性和重复性试验结果。该系统的性能,通过在不同的还原剂–还原剂摩尔比、表面活性剂类型、金属和表面活性剂浓度、合成温度和升温速率下合成的商用Pd/Al2O3和氧化钴纳米粒子的一氧化碳氧化反应进行评估。
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