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Screening of textile finishing agents available on the Chinese market: An important source of per- and polyfluoroalkyl substances to the environment

Mehvish Mumtaz, Yixiang Bao, Wenchao Li, Lingxiao Kong, Jun Huang, Gang Yu

《环境科学与工程前沿（英文）》 2019年 第13卷 第5期 doi: 10.1007/s11783-019-1145-0

摘要： Kendrick mass defect was used for PFASs screening in textile finishing agents (TFAs). Total oxidizable precursor assay provides insight into unknown precursors. Perfluorooctane sulfonate was found as impurity in short ECF technology based TFAs. Perfluorooctanoate was also detected in C6 telomerization based TFAs. Long chain precursors were also observed in both types of TFAs. Organofluorinated surfactants are widely employed in textile finishing agents (TFAs) to achieve oil, water, and stain repellency. This has been regarded as an important emission source of per-and polyfluoroalkyl substances (PFASs) to the environment. China is the biggest manufacturer of clothes, and thus TFA production is also a relevant industrial activity. Nevertheless, to date, no survey has been conducted on PFAS contents in commercially available TFAs. In the present study, TFA products were investigated by the Kendrick mass defect method. The quantification results demonstrated a significant presence of perfluorooctane sulfonate (0.37 mg/L) in TFAs manufactured by electrochemical fluorination technology. The products obtained by short-chain PFAS-based telomerization were dominated by perfluorooctanoic acid (mean concentration: 0.29 mg/L), whose values exceeded the limits stated in the European Chemical Agency guidelines (0.025 mg/L). Moreover, the total oxidizable precursor assay indicated high levels of indirectly quantified precursors with long alkyl chains (C7–C9). Together, these results suggest that there is currently a certain of environmental and health risks in China that originates from the utilization of TFAs, and a better manufacturing processes are required to reduce such risks.

关键词： Textile finishing agents     Kendrick mass defect     Total oxidizable precursor assay    

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Acoustic fault signal extraction via the line-defect phononic crystals

《机械工程前沿（英文）》 2022年 第17卷 第1期   页码 10-10 doi: 10.1007/s11465-021-0666-y

摘要： Rotating machine fault signal extraction becomes increasingly important in practical engineering applications. However, fault signals with low signal-to-noise ratios (SNRs) are difficult to extract, especially at the early stage of fault diagnosis. In this paper, 2D line-defect phononic crystals (PCs) consisting of periodic acrylic tubes with slit are proposed for weak signal detection. The defect band, namely, the formed resonance band of line-defect PCs enables the incident acoustic wave at the resonance frequency to be trapped and enhanced at the resonance cavity. The noise can be filtered by the band gap. As a result, fault signals with high SNRs can be obtained for fault feature extraction. The effectiveness of weak harmonic and periodic impulse signal detection via line-defect PCs are investigated in numerical and experimental studies. All the numerical and experimental results indicate that line-defect PCs can be well used for extracting weak harmonic and periodic impulse signals. This work will provide potential for extracting weak signals in many practical engineering applications.

关键词： phononic crystals     line-defect     fault signal extraction     acoustic enhancement    

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Research progress of defect-engineered UiO-66(Zr) MOFs for photocatalytic hydrogen production

《能源前沿（英文）》 2021年 第15卷 第3期   页码 656-666 doi: 10.1007/s11708-021-0765-9

摘要： In recent years, defect-engineered Zr-based UiO-66 metal-organic frameworks (UiO-66(Zr) metal-organic frameworks (MOFs)) have shown huge advantages in catalytic, functional materials, adsorption, and other fields due to their large surface areas, well-ordered porous structures, and flexible tailorability. It is extremely challenging to introduce defect sites in the synthesis of MOFs to regulate the physicochemical properties of materials such as (energy band structure, pore structure, etc.) to obtain an excellent performance. This paper reviews the recent research results of synthesis methods, characterization technologies, and application fields of defect-engineered UiO-66(Zr) MOFs materials in order to provide new insights to synthesize high-performance UiO-66(Zr) MOFs materials and promote the development of UiO-66(Zr) in various fields.

关键词： defect engineering     metal-organic frameworks     UiO-66     photocatalysis    

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The defect-length effect in corrosion detection with magnetic method for bridge cables

Qiwei ZHANG, Rongya XIN

《结构与土木工程前沿（英文）》 2018年 第12卷 第4期   页码 662-671 doi: 10.1007/s11709-018-0512-4

摘要：

Quantitative evaluation of the steel corrosion in cables is significant for the safe operation of cable-supported bridges. The magnetic flux (MF) examination shows great potential to detect the corrosion defect, or loss of metallic cross-sectional area (LMA). An LMA defect in steel cables can be measured accurately when it is longer than a certain length. However, for defects in early stage, where the length of corrosion area is short, the MF examination may produce unacceptable error. In this study, the effect of defect length on the MF examination for corrosion detection of bridge cables is investigated through theoretical analysis and model experiments. An original analytical model to quantify the influence of defect length is proposed based on the equivalent magnetic circuit method. Then, MF examination experiments are performed on a series of cable models with different defect lengths and locations to verify the analytical model. Further, parameter study is conducted based on the proposed analytical model to clarify the mechanism of the defect-length effect. The results show that the area loss caused by short corrosion damage will be underestimated if the defect-length effect is neglected, and this effect can be quantified efficiently with the proposed analytical model.

关键词： bridge cable     corrosion detection     defect length     MF examination     quantitative evaluation    

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Single-electromagnet levitation for density measurement and defect detection

Yuhan JIA, Peng ZHAO, Jun XIE, Xuechun ZHANG, Hongwei ZHOU, Jianzhong FU

《机械工程前沿（英文）》 2021年 第16卷 第1期   页码 186-195 doi: 10.1007/s11465-020-0608-0

摘要： This paper presents a single-electromagnet levitation device to measure the densities and detect the internal defects of antimagnetic materials. The experimental device has an electromagnet in its lower part and a pure iron core in the upper part. When the electromagnet is activated, samples can be levitated stably in a paramagnetic solution. Compared with traditional magnetic levitation devices, the single-electromagnet levitation device is adjustable. Different currents, electromagnet shapes, and distances between the electromagnet and iron core are used in the experiment depending on the type of samples. The magnetic field formed by the electromagnet is strong. When the concentration of the MnCl aqueous solution is 3 mol/L, the measuring range of the single-electromagnet levitation device ranges from 1.301 to 2.308 g/cm . However, with the same concentration of MnCl aqueous solution (3 mol/L), the measuring range of a magnetic levitation device built with permanent magnets is only from 1.15 to 1.50 g/cm . The single-electromagnet levitation device has a large measuring range and can realize accurate density measurement and defect detection of high-density materials, such as glass and aluminum alloy.

关键词： single-electromagnet     electromagnetic levitation     density measurement     defect detection    

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Statistical analysis of recombination properties of the boron-oxygen defect in p-type Czochralski silicon

Nitin NAMPALLI,Tsun Hang FUNG,Stuart WENHAM,Brett HALLAM,Malcolm ABBOTT

《能源前沿（英文）》 2017年 第11卷 第1期   页码 4-22 doi: 10.1007/s11708-016-0442-6

摘要： This paper presents the application of lifetime spectroscopy to the study of carrier-induced degradation ascribed to the boron-oxygen (BO) defect. Specifically, a large data set of p-type silicon samples is used to investigate two important aspects of carrier lifetime analysis: ① the methods used to extract the recombination lifetime associated with the defect and ② the underlying assumption that carrier injection does not affect lifetime components unrelated to the defect. The results demonstrate that the capture cross section ratio associated with the donor level of the BO defect ( ) vary widely depending on the specific method used to extract the defect-specific recombination lifetime. For the data set studied here, it was also found that illumination used to form the defect caused minor, but statistically significant changes in the surface passivation used. This violation of the fundamental assumption could be accounted for by applying appropriate curve fitting methods, resulting in an improved estimate of (11.90±0.45) for the fully formed BO defect when modeled using the donor level alone. Illumination also appeared to cause a minor, apparently injection-independent change in lifetime that could not be attributed to the donor level of the BO defect alone and is likely related to the acceptor level of the BO defect. While specific to the BO defect, this study has implications for the use of lifetime spectroscopy to study other carrier induced defects. Finally, we demonstrate the use of a unit-less regression goodness-of-fit metric for lifetime data that is easy to interpret and accounts for repeatability error.

关键词： Czochralski silicon     boron-oxygen defect     injection dependent lifetime spectroscopy     goodness-of-fit     repeatability error    

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桥面铺装病害检测技术研究

郭成超,许朋飞,崔璨

《中国工程科学》 2017年 第19卷 第6期   页码 38-43 doi: 10.15302/J-SSCAE-2017.06.006

摘要：

在桥梁的全生命周期中，桥面板是最容易出现病害的部分。桥面铺装层常常由于施工方法选择不当、混凝土老化、钢筋锈蚀等原因产生各种病害，这对桥梁结构、使用性能都会造成不利影响，因此有必要对相关病害进行检测，并对桥面质量做出相关评价。本文介绍了国内外四种主要无损检测方法（半电池电位法、探地雷达法、冲击回波法、红外热成像法）的工作原理以及相应的检测设备，利用其中一种或几种方法能准确评估桥面板的恶化情况，对桥面板状况进行快速、无损检测，为实现桥面铺装的准确检测提供技术支持，从而减少结构病害，延长桥梁的使用寿命。

关键词： 桥面铺装     病害     无损检测    

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Effect of cavity defect on the triaxial mechanical properties of high-performance concrete

Yanbin ZHANG; Zhe WANG; Mingyu FENG

《结构与土木工程前沿（英文）》 2022年 第16卷 第5期   页码 600-614 doi: 10.1007/s11709-022-0821-5

摘要： The stress concentration of pipe structure or cavity defect has a great effect on the mechanical properties of the high-performance concrete (HPC) members in deep underground locations. However, the behaviour of HPC with cavities under triaxial compression is not understood, especially when pressurized liquid flows into the fractures from the cavity. This study aims to investigate the effect of the cavity and the confining pressure on the failure mechanisms, strengths, and deformation properties of HPC with a new experimental scheme. In this experiment, the pressurized liquid can only contact the surface of the sample in the cavity, while the other surfaces are isolated from the pressurized liquid. To further explore the effect of the cavity, the same experiments are also conducted on sealed and unsealed intact samples without a cavity. The failure modes and stress-strain curves of all types of the samples are presented. Under various confining pressures, all the samples with a cavity suffer shear failure, and there are always secondary tensile fractures initiating from the cavity sidewall. Additionally, it can be determined from the failure modes and the stress-strain curves that the shear fractures result from the sidewall failure. Based on the different effects of the cavity on the lateral deformations in different directions, the initiation of the sidewall fracture is well predicted. The experimental results show that both the increase of the confining pressure and the decrease of the cavity size are conducive to the initiation of sidewall fracture. Moreover, the cavity weakens the strength of the sample, and this study gives a modified Power-law criterion in which the cavity size is added as an impact factor to predict the strength of the sample.

关键词： high-performance concrete     cavity     conventional triaxial compression     pressurized liquid     modified power-law criterion    

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Construction of defect-containing UiO-66/MoSe heterojunctions with superior photocatalytic performance

《化学科学与工程前沿（英文）》 2023年 第17卷 第4期   页码 449-459 doi: 10.1007/s11705-022-2226-3

摘要： Metal–organic frameworks are recognized as promising multifunctional materials, especially metal–organic framework-based photocatalysts, which are considered to be ideal photocatalytic materials. Herein, a new type of UiO-66/MoSe2 composite was prepared using the solvothermal method. The optimum composite was selected by adjusting the mass ratio of UiO-66 and MoSe2. X-ray diffraction analysis showed that the mass ratio influenced the crystal plane exposure rate of the composite, which may have affected its photocatalytic performance. The composite is composed of ultra-thin flower-like MoSe2 that wrapped around cubic UiO-66, a structure that increases the abundance of active sites for reactions and is more conducive to the separation of carriers. The photocatalytic properties of the composite were evaluated by measuring the degradation rate of Rhodamine B and the catalyst’s ability to reduce Cr(VI)-containing wastewater under visible light irradiation. Rhodamine B was decolorized completely in 120 min, and most of the Cr(VI) was reduced within 150 min. The photochemical mechanism of the complex was studied in detail. The existence of Mo6+ and oxygen vacancies, in addition to the Z-type heterojunction promote the separation of electrons and holes, which enhances the photocatalytic effect.

关键词： UiO-66/MoSe2     photocatalysis     dye-containing wastewater     heavy metal wastewater     oxygen vacancies    

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Thermo-fluidic devices and materials inspired from mass and energy transport phenomena in biological

Jian XIAO , Jing LIU ,

《能源前沿（英文）》 2009年 第3卷 第1期   页码 47-59 doi: 10.1007/s11708-008-0068-4

摘要： Mass and energy transport consists of one of the most significant physiological processes in nature, which guarantees many amazing biological phenomena and activities. Borrowing such idea, many state-of-the-art thermo-fluidic devices and materials such as artificial kidneys, carrier erythrocyte, blood substitutes and so on have been successfully invented. Besides, new emerging technologies are still being developed. This paper is dedicated to presenting a relatively complete review of the typical devices and materials in clinical use inspired by biological mass and energy transport mechanisms. Particularly, these artificial thermo-fluidic devices and materials will be categorized into organ transplantation, drug delivery, nutrient transport, micro operation, and power supply. Potential approaches for innovating conventional technologies were discussed, corresponding biological phenomena and physical mechanisms were interpreted, future promising mass-and-energy-transport-based bionic devices were suggested, and prospects along this direction were pointed out. It is expected that many artificial devices based on biological mass and energy transport principle will appear to better improve various fields related to human life in the near future.

关键词： bionics     mass transport     energy transport     artificial devices and materials     biology system     nature phenomena     medical device.    

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Convective mass transfer from a horizontal rotating cylinder in a slot air jet flow

Hongting MA , Dandan MA , Na YANG ,

《能源前沿（英文）》 2009年 第3卷 第3期   页码 289-296 doi: 10.1007/s11708-009-0019-8

摘要： The effects of air jet impinging on the mass transfer characteristics from a rotating spinning cylinder surface were experimentally investigated. The effects of rotational Reynolds number

关键词： air jet impinging     rotating cylinder     critical point     mass transfer characteristics    

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Parametric control of structural responses using an optimal passive tuned mass damper under stationary

Min-Ho CHEY, Jae-Ung KIM

《结构与土木工程前沿（英文）》 2012年 第6卷 第3期   页码 267-280 doi: 10.1007/s11709-012-0170-x

摘要： In this study, the structural control strategy utilizing a passive tuned mass damper (TMD) system as a seismic damping device is outlined, highlighting the parametric optimization approach for displacement and acceleration control. The theory of stationary random processes and complex frequency response functions are explained and adopted. For the vibration control of an undamped structure, the optimal parameters of a TMD, such as the optimal tuning frequency and optimal damping ratio, to stationary Gaussian white noise acceleration are investigated by using a parametric optimization procedure. For damped structures, a numerical searching technique is used to obtain the optimal parameters of the TMD, and then the explicit formulae for these optimal parameters are derived through a sequence of curve-fitting schemes. Using these specified optimal parameters, several different controlled responses are examined, and then the displacement and acceleration based control effectiveness indices of the TMD are examined from the view point of RMS values. From the viewpoint of the RMS values of displacement and acceleration, the optimal TMDs adopted in this study shows clear performance improvements for the simplified model examined, and this means that the effective optimization of the TMD has a good potential as a customized target response-based structural strategy.

关键词： tuned mass damper     parametric optimization     passive control     white noise     earthquake excitation    

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Numerical modeling of mass transfer processes coupling with reaction for the design of the ozone oxidation

Hong Li, Fang Yi, Xingang Li, Xin Gao

《化学科学与工程前沿（英文）》 2021年 第15卷 第3期   页码 602-614 doi: 10.1007/s11705-020-1963-4

摘要： A computational model for an ozone oxidation column reactor used in dyeing wastewater treatment is proposed to represent, simulate, and predict the ozone bubble process. Considering the hydrodynamics, mass transfer, and ozone oxidation reaction, coupling modeling can more realistically calculate the ozone oxidation bubble process than the splitting methods proposed in previous research. The modeling is validated and shows great consistency with experimental data. The verified model is used to analyze the effect of operating conditions, such as the initial gas velocity and the ozone concentration, and structural conditions, such as multiple gas inlets. The ozone consumption is influenced by the gas velocity and the initial ozone concentration. The ozone’s utilization decreases with the increasing gas velocity while nearly the same at different initial ozone concentrations. Simulation results can be used in guiding the practical operation of dyeing wastewater treatment and in other ozonation systems with known rate constants in wastewater treatment.

关键词： ozone     wastewater treatment     numerical simulation     mass transfer    

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Simulation of blast induced crater in jointed rock mass by discontinuous deformation analysis method

Youjun NING, Xinmei AN, Jun YANG, Guowei MA,

《结构与土木工程前沿（英文）》 2010年 第4卷 第2期   页码 223-232 doi: 10.1007/s11709-010-0022-5

摘要： Rock blasting is a dynamic process accompanied with the propagations of shock waves and the dispersion of the explosion gas. This paper adopts the discontinuous deformation analysis (DDA) method to simulate the rock blasting process. A dynamic parameter adjustment and the non-reflecting boundary condition are implemented in the DDA method. The sub-block DDA method to simulate fracture problems is used. The blasting process in jointed rock mass is simulated by application of the explosion gas pressure on the expanding borehole walls and induced connected fracture surfaces around the boreholes. The blast craters with different overburdens are derived. The whole process including the explosion gas dispersion, borehole expansion, rock mass failure and cast, and the formation of the final blasting piles in rock blasting are well reproduced numerically. Parametric study for different overburdens is carried out, and the results are analyzed and discussed.

关键词： blast crater     jointed rock mass     explosion gas pressure     discontinuous deformation analysis (DDA) method    

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一种面向软件缺陷预测的相似性度量特征选择方法 Article

Qiao YU, Shu-juan JIANG, Rong-cun WANG, Hong-yang WANG

《信息与电子工程前沿（英文）》 2017年 第18卷 第11期   页码 1744-1753 doi: 10.1631/FITEE.1601322

摘要： 软件缺陷预测旨在通过历史数据和能反映软件模块特性的软件特征来发现潜在缺陷。然而，有的特征可能与类别（有缺陷或无缺陷）的相关性较高，有的特征可能是冗余的或无关的。针对软件缺陷预测中不同特征与类别的相关性差异，本文提出一种基于相似性度量（similarity measure, SM）的特征选择方法。首先，根据不同类样本间的相似性来更新特征权重；然后，按照特征权重值降序排列生成特征排序列表，并依次选取特征排序列表中的所有特征子集；最后，在KNN（k-nearest neighbor）模型上验证所有特征子集的分类性能，并采用AUC （area under curve）指标进行度量。在11个美国航空航天局（NASA）数据集上进行实验验证，结果表明，与其它四种特征选择方法相比，本文方法具有与之相当甚至更高的分类性能。

关键词： 软件缺陷预测；特征选择；相似性度量；特征权重；特征排序列表    

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标题 作者 时间 类型 操作

Screening of textile finishing agents available on the Chinese market: An important source of per- and polyfluoroalkyl substances to the environment

Mehvish Mumtaz, Yixiang Bao, Wenchao Li, Lingxiao Kong, Jun Huang, Gang Yu

期刊论文

Acoustic fault signal extraction via the line-defect phononic crystals

期刊论文

Research progress of defect-engineered UiO-66(Zr) MOFs for photocatalytic hydrogen production

期刊论文

The defect-length effect in corrosion detection with magnetic method for bridge cables

Qiwei ZHANG, Rongya XIN

期刊论文

Single-electromagnet levitation for density measurement and defect detection

Yuhan JIA, Peng ZHAO, Jun XIE, Xuechun ZHANG, Hongwei ZHOU, Jianzhong FU

期刊论文

Statistical analysis of recombination properties of the boron-oxygen defect in p-type Czochralski silicon

Nitin NAMPALLI,Tsun Hang FUNG,Stuart WENHAM,Brett HALLAM,Malcolm ABBOTT

期刊论文

桥面铺装病害检测技术研究

郭成超,许朋飞,崔璨

期刊论文

Effect of cavity defect on the triaxial mechanical properties of high-performance concrete

Yanbin ZHANG; Zhe WANG; Mingyu FENG

期刊论文

Construction of defect-containing UiO-66/MoSe heterojunctions with superior photocatalytic performance

期刊论文

Thermo-fluidic devices and materials inspired from mass and energy transport phenomena in biological

Jian XIAO , Jing LIU ,

期刊论文

Convective mass transfer from a horizontal rotating cylinder in a slot air jet flow

Hongting MA , Dandan MA , Na YANG ,

期刊论文

Parametric control of structural responses using an optimal passive tuned mass damper under stationary

Min-Ho CHEY, Jae-Ung KIM

期刊论文

Numerical modeling of mass transfer processes coupling with reaction for the design of the ozone oxidation

Hong Li, Fang Yi, Xingang Li, Xin Gao

期刊论文

Simulation of blast induced crater in jointed rock mass by discontinuous deformation analysis method

Youjun NING, Xinmei AN, Jun YANG, Guowei MA,

期刊论文

一种面向软件缺陷预测的相似性度量特征选择方法

Qiao YU, Shu-juan JIANG, Rong-cun WANG, Hong-yang WANG

期刊论文