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2009, Volume 3, Issue 2

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Frontiers of Chemical Science and Engineering >> 2009, Volume 3, Issue 2 doi: 10.1007/s11705-009-0059-y

Study on a green synthetic method of TRPPMCl (M= Fe, Mn, Co)

Institute of Green Chemistry and Fine Chemicals, Beijing University of Technology, Beijing 100124, China

Available online: 2009-06-05
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Abstract

A green synthetic method using mixted solvents of di-methyl formamide(DMF) and acids instead of single DMF to synthesize metalloporphyrins(TRPPMCl) from TRPPH and MCl metallization was proposed in this paper. A series of TRPPMCl (M= Fe, Mn, Co) were synthesized through this innovative synthetic method, and these complexes were characterized with various spectroscopic techniques, including IR and UV-Vis spectroscopy. The results showed that the metallization time was markedly reduced from about 10 h to 0.5 h in contrast with the conventional synthetic methods.

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