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利用Nd-Fe-B 油泥回收制备高性能烧结磁体的有效方法 Article

尹小文, 岳明, 路清梅, 刘敏, 王峰, 邱玉冰, 刘卫强, 左铁镛, 查善顺, 李绪亮, 衣晓飞

《工程（英文）》 2020年 第6卷 第2期   页码 165-172 doi: 10.1016/j.eng.2019.11.007

摘要：

全球稀土储量的下降以及当前湿法回收技术对环境造成的影响日益受到人们的关注，开发一种有效回收钕铁硼（Nd-Fe-B）烧结磁体生产过程中剩余油泥的技术已迫在眉睫。本研究选择了Nd-Fe-B烧结磁体加工过程中产生的无心磨削油泥作为原材料。我们对油泥进行了还原扩散（RD）处理，以合成可供回收的钕磁体（Nd2Fe14B）粉末。通过调节反应温度和油泥中的钙含量，我们系统地研究了Nd-Fe-B油泥回收过程中的反应机理。我们在回收的Nd2Fe14B颗粒中掺杂了含量为37.7 wt%的Nd4Fe14B粉末，用以制备Nd-Fe-B烧结磁体

关键词： Nd-Fe-B磨削油泥     再生烧结磁体     钙还原扩散     富稀土合金掺杂    

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各向异性热压稀土永磁体的热变形机制及微磁结构研究

李卫,朱明刚

《中国工程科学》 2011年 第13卷 第10期   页码 4-12

摘要：

重点研究制备工艺对各向异性热压稀土永磁体性能的影响，探讨了热压永磁体的热变形机理和数学描述模型，并尝试从微磁结构的角度研究各向异性纳米晶Nd-Fe-B获得了最佳磁性能为：Hcj=1 157 kA/m，Br=1.465 T，(BH)max=426 kJ/m3纳米晶Nd-Fe-B磁体。

关键词： 纳米晶Nd-Fe-B辐向环     热压－热变形     各向异性     微磁结构    

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快速热处理制备纳米耦合Nd-Fe-B磁体的结构与磁性能研究 Review

杨金波, 韩景智, 田海东, 查亮, 张雄祚, 金哲星, 梁栋, 杨文云, 刘顺荃, 王常生

《工程（英文）》 2020年 第6卷 第2期   页码 131-139 doi: 10.1016/j.eng.2019.12.008

摘要： 在本工作中，我们总结了快速热处理技术——电子束曝光，对Nd12.5-xFe80.8+xB相比于传统退火技术所需的退火晶化时间（15 min），电子束曝光下结晶时间仅需0.1 s，并且所需结晶温度降低约248 ℃（Nd2Fe14B单相材料）。在电子束曝光条件下，还观察到Nd2Fe14B和α-Fe相协同晶化效应。随着Fe含量的增加，协同晶化的影响变得更加明显。由于电子束曝光下协同晶化改善了Nd2Fe14B和α-Fe相的均匀性以及抑制了晶粒的过度生长，因而电子束曝光相比于传统退火技术使材料获得了更加优异的磁性能

关键词： 纳米耦合     电子束曝光     朗道和郎之万动力学模拟     协同晶化    

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Carbon nanotubes-incorporated MIL-88B-Fe as highly efficient Fenton-like catalyst for degradation of

Hang Zhang, Shuo Chen, Haiguang Zhang, Xinfei Fan, Cong Gao, Hongtao Yu, Xie Quan

《环境科学与工程前沿（英文）》 2019年 第13卷 第2期 doi: 10.1007/s11783-019-1101-z

摘要：

CNTs were incorporated into MIL-88B-Fe to get a new Fenton-like catalyst (C@M).

Fe(II) was introduced in C@M to get a fast initiation of Fenton-like reaction.

Fe(II) content in C@M was related with oxygen-containing functional groups on CNTs.

C@M shows efficient catalytic degradation of pollutants over a wide pH range.

关键词： Heterogeneous Fenton-like catalysts     MIL-88B-Fe     CNTs     Organic pollutants     Mechanism    

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The performance of nitrate-reducing Fe(II) oxidation processes under variable initial Fe/N ratios: The

《环境科学与工程前沿（英文）》 2021年 第15卷 第4期 doi: 10.1007/s11783-020-1366-2

摘要：

•Bacterially-mediated coupled N and Fe processes examined in incubation experiments.

关键词： Denitrification     N2O emission     Fe(II) oxidation     Fe/N ratio     Fe minerals    

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结构功能一体化的高性能陶瓷材料的研究与开发

江东亮

《中国工程科学》 2003年 第5卷 第2期   页码 35-39

摘要：

从当前新材料的开发和材料科学发展向多功能、小型化、复合化、低成本制备等要求出发, 并就现有高性能陶瓷材料的基本性能和材料制备工艺上的优缺点进行了分析；简要介绍了碳化硅(SiC)陶瓷、 添加Nd的钇铝石榴子石(Nd-YAG)陶瓷、掺有稀土的氮化硅(RE-Si3N4)陶瓷等几种具有结构和功能一体化高性能陶瓷材料的优良性能,可能的应用以及目前存在的问题,特别是在基础研究和制备科学上今后应予以关注的方面

关键词： 结构和功能一体化     高性能陶瓷     碳化硅     Nd-YAG     RE-Si3N4    

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Cadmium removal mechanistic comparison of three Fe-based nanomaterials: Water-chemistry and roles ofFe dissolution

《环境科学与工程前沿（英文）》 2022年 第16卷 第12期 doi: 10.1007/s11783-022-1586-8

摘要：

● nZVI, S-nZVI, and nFeS were systematically compared for Cd(II) removal.

关键词： Nano zero valent iron     Sulfided zero valent iron     FeS     Cd(II) immobilization     Fe dissolution    

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Fertilizer drawn forward osmosis as an alternative to 2nd pass seawater reverse osmosis: Estimation of

《环境科学与工程前沿（英文）》 2021年 第15卷 第6期 doi: 10.1007/s11783-021-1428-0

摘要：

• The boron concentration in diluted DS can satisfy the irrigation water standard.

关键词： Fertilizer drawn forward osmosis (FDFO)     Boron removal     Specific energy consumption (SEC)     Seawater reverse osmosis (SWRO)     Irrigation water production    

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Synergistic effect of V and Fe in Ni/Fe/V ternary layered double hydroxides for efficient and durable

《化学科学与工程前沿（英文）》 2023年 第17卷 第1期   页码 102-115 doi: 10.1007/s11705-022-2179-6

摘要： High-performance and stable electrocatalysts are vital for the oxygen evolution reaction (OER). Herein, via a one-pot hydrothermal method, Ni/Fe/V ternary layered double hydroxides (NiFeV-LDH) derived from Ni foam are fabricated to work as highly active and durable electrocatalysts for OER. By changing the feeding ratio of Fe and V salts, the prepared ternary hydroxides were optimized. At an Fe:V ratio of 0.5:0.5, NiFeV-LDH exhibits outstanding OER activity superior to that of the binary hydroxides, requiring overpotentials of 269 and 274 mV at 50 mA·cm–2 in the linear sweep voltammetry and sampled current voltammetry measurements, respectively. Importantly, NiFeV-LDH shows extraordinary long-term stability (≥ 75 h) at an extremely high current density of 200 mA·cm–2. In contrast, the binary hydroxides present quick decay at 200 mA·cm–2 or even reduced current densities (150 and 100 mA·cm–2). The outstanding OER performance of NiFeV-LDH benefits from the synergistic effect of V and Fe while doping the third metal into bimetallic hydroxide layers: (a) Fe plays a crucial role as the active site; (b) electron-withdrawing V stabilizes the high valence state of Fe, thus accelerating the OER process; (c) V further offers great stabilization for the formed intermediate of FeOOH, thus achieving superior durability.

关键词： oxygen evolution reaction     electrocatalysts     ternary layered double hydroxides     long-term stability    

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Floret-like Fe–N nanoparticle-embedded porous carbon superstructures from a Fe-covalent triazine polymer

《化学科学与工程前沿（英文）》 2023年 第17卷 第5期   页码 525-535 doi: 10.1007/s11705-022-2232-5

摘要： Fe–Nx nanoparticles-embedded porous carbons with a desirable superstructure have attracted immense attention as promising catalysts for electrochemical oxygen reduction reaction. Herein, we employed Fe-coordinated covalent triazine polymer for the fabrication of Fe–Nx nanoparticle-embedded porous carbon nanoflorets (Fe/N@CNFs) employing a hypersaline-confinement-conversion strategy. Presence of tailored N types within the covalent triazine polymer interwork in high proportions contributes to the generation of Fe/N coordination and subsequent Fe–Nx nanoparticles. Owing to the utilization of NaCl crystals, the resultant Fe/N@CNF-800 which was generated by pyrolysis at 800 °C showed nanoflower structure and large specific surface area, which remarkably suppressed the agglomeration of high catalytic active sites. As expect, the Fe/N@CNF-800 exhibited unexpected oxygen reduction reaction catalytic performance with an ultrahigh half-wave potential (0.89 V vs. reversible hydrogen electrode), a dominant 4e– transfer approach and great cycle stability (> 92% after 100000 s). As a demonstration, the Fe/N-PCNF-800-assembled zinc–air battery delivered a high open circuit voltage of 1.51 V, a maximum peak power density of 164 mW·cm–2, as well as eminent rate performance, surpassing those of commercial Pt/C. This contribution offers a valuable avenue to exploit efficient metal nanoparticles-based carbon catalysts towards energy-related electrocatalytic reactions and beyond.

关键词： Fe–Nx nanoparticles     hypersaline-confinement conversion     floret-like carbon     covalent triazine polymers     oxygen reduction reaction    

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Ni-Bi 助剂用于α-Fe2O3 Letter

党珂,王拓,李澄澄,张冀杰,刘珊珊,巩金龙

《工程（英文）》 2017年 第3卷 第3期   页码 285-289 doi: 10.1016/J.ENG.2017.03.005

摘要：

本文提出了镍-硼酸(Ni-Bi) 助催化剂负载于α 型三氧化二铁(Fe2O3) 具有提升表面动力学和钝化表面态的双重作用Ni-Bi助剂的负载使Fe2O3 光电阳极的光电流起始电位产生230 mV 的负移，1.23 V(vs.Ni-Bi助剂层中的Bi 促进了产氧反应的脱质子步骤。

关键词： 镍-硼酸     &alpha     型三氧化二铁     产氧反应     助催化剂    

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Solid-state-reaction fabrication and properties of a high-doping Nd:YAG transparent laser ceramic

WU Yusong, LI Jiang, PAN Yubai, LIU Wenbin, AN Liqiong, WANG Shiwei, GUO Jingkun

《化学科学与工程前沿（英文）》 2008年 第2卷 第3期   页码 248-252 doi: 10.1007/s11705-008-0048-6

摘要： High-quality neodymium-doped yttrium aluminum garnet (Nd:YAG) transparent ceramic (4.0 mole percent) was fabricated by a solid-state reaction method and vacuum sintering. The microstructure, optical transmittance, spectral properties and laser performance were investigated. The average grain size of the sample is about 10 ?m. The transmittance of a 2.8-mm thick sample reaches 79.5% at the laser wavelength of 1064 nm. The highest absorption peak is centered at 807 nm and the absorption coefficient is 13.9 cm. The absorption coefficient at the laser wavelength is 0.2 cm. The main emission peak is at 1064 nm and the fluorescence lifetime is 102 ?s. A laser diode (808 nm) whose maximum output is about 1000 mW was used as a pump source and an end-pumped laser experiment was performed. The 1064 nm-CW-laser output was obtained and the threshold is 733 mW. With 998 mW of maximum absorbed pump power, a laser output of 17 mW is obtained with a slope efficiency of 6.1%.

关键词： neodymium-doped yttrium     maximum absorbed     microstructure     fluorescence lifetime     threshold    

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Hybrid genetic algorithm for bi-objective resource-constrained project scheduling

Fikri KUCUKSAYACIGIL, Gündüz ULUSOY

《工程管理前沿（英文）》 2020年 第7卷 第3期   页码 426-446 doi: 10.1007/s42524-020-0100-x

摘要： In this study, we considered a bi-objective, multi-project, multi-mode resource-constrained project scheduling problem. We adopted three objective pairs as combinations of the net present value (NPV) as a financial performance measure with one of the time-based performance measures, namely, makespan ( ), mean completion time (MCT), and mean flow time (MFT) (i.e., min /max , min /max , and min /max ). We developed a hybrid non-dominated sorting genetic algorithm II (hybrid-NSGA-II) as a solution method by introducing a backward–forward pass (BFP) procedure and an injection procedure into NSGA-II. The BFP was proposed for new population generation and post-processing. Then, an injection procedure was introduced to increase diversity. The BFP and injection procedures led to improved objective functional values. The injection procedure generated a significantly high number of non-dominated solutions, thereby resulting in great diversity. An extensive computational study was performed. Results showed that hybrid-NSGA-II surpassed NSGA-II in terms of the performance metrics hypervolume, maximum spread, and the number of non-dominated solutions. Solutions were obtained for the objective pairs using hybrid-NSGA-II and three different test problem sets with specific properties. Further analysis was performed by employing cash balance, which was another financial performance measure of practical importance. Several managerial insights and extensions for further research were presented.

关键词： backward–forward scheduling     hybrid bi-objective genetic algorithm     injection procedure     maximum cash balance     multi-objective multi-project multi-mode resource-constrained project scheduling problem    

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Catalytic process modeling and sensitivity analysis of alkylation of benzene with ethanol over MIL-101(Fe) and MIL-88(Fe)

Ehsan Rahmani, Mohammad Rahmani

《化学科学与工程前沿（英文）》 2020年 第14卷 第6期   页码 1100-1111 doi: 10.1007/s11705-019-1891-3

摘要： A solvothermal method was used to synthesize MIL-101(Fe) and MIL-88(Fe), which were used for alkylation of benzene. The synthesized catalysts were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, field emission scanning electron microscope, dynamic light scattering, and BET techniques. Metal-organic frameworks (MOFs) were modeled to investigate the catalytic performance and existence of mass transfer limitations. Calculated effectiveness factors revealed absence of internal and external mass transfer. Sensitivity analysis revealed best operating conditions over MIL-101 at 120°C and 5 bar and over MIL-88 at 142°C and 9 bar.

关键词： MOFs     alkylation     ethylbenzene     catalysts pellet model     kinetic model     sensitivity analysis    

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Effect of Fe on NO release during char combustion in air and O

Ying GU, Xiaowei LIU, Bo ZHAO, Minghou XU

《能源前沿（英文）》 2012年 第6卷 第2期   页码 200-206 doi: 10.1007/s11708-012-0181-2

摘要： The chemistry of char was probed by studying nitrogen release under the reactions with air and oxy-fuel combustion. The experiments were conducted in a drop tube furnace and a fixed bed flow reactor. NO was observed during those experiments. The results show that the particle size of char generated at 1073 K in CO is larger than that in N . However, at 1573 K, it is smaller in CO atmosphere due to particle breaking by gasification of char and CO . The Fe addition increases the NO conversion ratio, and the effect of Fe rises steeply with the process going until it becomes stable in the end. The results also indicate that the release of NO increases more significantly with the Fe addition in oxy-fuel environment.

关键词： NO     Fe     char     combustion     CO2    

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标题 作者 时间 类型 操作

利用Nd-Fe-B 油泥回收制备高性能烧结磁体的有效方法

尹小文, 岳明, 路清梅, 刘敏, 王峰, 邱玉冰, 刘卫强, 左铁镛, 查善顺, 李绪亮, 衣晓飞

期刊论文

各向异性热压稀土永磁体的热变形机制及微磁结构研究

李卫,朱明刚

期刊论文

快速热处理制备纳米耦合Nd-Fe-B磁体的结构与磁性能研究

杨金波, 韩景智, 田海东, 查亮, 张雄祚, 金哲星, 梁栋, 杨文云, 刘顺荃, 王常生

期刊论文

Carbon nanotubes-incorporated MIL-88B-Fe as highly efficient Fenton-like catalyst for degradation of

Hang Zhang, Shuo Chen, Haiguang Zhang, Xinfei Fan, Cong Gao, Hongtao Yu, Xie Quan

期刊论文

The performance of nitrate-reducing Fe(II) oxidation processes under variable initial Fe/N ratios: The

期刊论文

结构功能一体化的高性能陶瓷材料的研究与开发

江东亮

期刊论文

Cadmium removal mechanistic comparison of three Fe-based nanomaterials: Water-chemistry and roles ofFe dissolution

期刊论文

Fertilizer drawn forward osmosis as an alternative to 2nd pass seawater reverse osmosis: Estimation of

期刊论文

Synergistic effect of V and Fe in Ni/Fe/V ternary layered double hydroxides for efficient and durable

期刊论文

Floret-like Fe–N nanoparticle-embedded porous carbon superstructures from a Fe-covalent triazine polymer

期刊论文

Ni-Bi 助剂用于α-Fe2O3

党珂,王拓,李澄澄,张冀杰,刘珊珊,巩金龙

期刊论文

Solid-state-reaction fabrication and properties of a high-doping Nd:YAG transparent laser ceramic

WU Yusong, LI Jiang, PAN Yubai, LIU Wenbin, AN Liqiong, WANG Shiwei, GUO Jingkun

期刊论文

Hybrid genetic algorithm for bi-objective resource-constrained project scheduling

Fikri KUCUKSAYACIGIL, Gündüz ULUSOY

期刊论文

Catalytic process modeling and sensitivity analysis of alkylation of benzene with ethanol over MIL-101(Fe) and MIL-88(Fe)

Ehsan Rahmani, Mohammad Rahmani

期刊论文

Effect of Fe on NO release during char combustion in air and O

Ying GU, Xiaowei LIU, Bo ZHAO, Minghou XU

期刊论文