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Influence of entrainer recycle for batch heteroazeotropic distillation
Laszlo Hegely, Peter Lang
《化学科学与工程前沿(英文)》 2018年 第12卷 第4期 页码 643-659 doi: 10.1007/s11705-018-1760-5
Dehydration of isopropanol applying batch heteroazeotropic distillation with toluene as entrainer (E) is investigated. The composition of the feed is near to that of the isopropanol (A)-water (B) azeotrope. The effects of recycling the entrainer and the off-cut are studied by dynamic simulation with a professional flow-sheet simulator. Three consecutive batches (one production cycle) is studied. Both operational modes (Mode I: decantation after distillation and Mode II: decantation during distillation) are simulated. For Mode II, calculations are performed both for Strategy A (distillate from the aqueous (E-lean) phase only) and Strategy B (partial withdrawal of the organic (E-rich phase), as well). The E-rich phase, the final column hold-up and the off-cut (Mode II only) are recycled to the next batch. The influence of the following parameters are determined: quantity of entrainer, reflux ratios of the steps. The variations caused by the recycling in the 2nd and 3rd batches are also shown. The best results (lowest specific energy demand and highest recovery of A) are obtained by Mode II, Strategy A. Recycling increases the recovery, and drastically diminishes the entrainer consumption. However, it makes the production slower and decreases the quantity of fresh feed that can be processed.
关键词: batch distillation heteroazeotropic distillation operational policies off-cut recycle entrainer
Ao Yang, Yang Su, Tao Shi, Jingzheng Ren, Weifeng Shen, Teng Zhou
《化学科学与工程前沿(英文)》 2022年 第16卷 第2期 页码 303-315 doi: 10.1007/s11705-021-2044-z
关键词: extractive distillation solvent selection conceptual design process optimization heat integration
《化学科学与工程前沿(英文)》 2023年 第17卷 第1期 页码 34-45 doi: 10.1007/s11705-022-2234-3
关键词: ionic liquid entrainer screening feasibility analysis extractive distillation
标题 作者 时间 类型 操作
Influence of entrainer recycle for batch heteroazeotropic distillation
Laszlo Hegely, Peter Lang
期刊论文
Energy-efficient recovery of tetrahydrofuran and ethyl acetate by triple-column extractive distillation: entrainer
Ao Yang, Yang Su, Tao Shi, Jingzheng Ren, Weifeng Shen, Teng Zhou
期刊论文