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Optimization of the O/HO process with response surface methodology for pretreatment of mother liquor

《环境科学与工程前沿（英文）》 2021年第15卷第4期 doi: 10.1007/s11783-020-1371-5

摘要：

• Real ML-GFW with high salinity and high organics was degraded by O₃/H₂O₂ process.

关键词： High salinity High organic matters Gas field wastewater O₃/H₂O₂ Response surface methodology

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造纸提取黑液污染零排放新工艺研究

黄立新,钟运猷,韩磊,王占军,唐金鑫,王宗濂,周瑞君,周荣

《中国工程科学》 2001年第3卷第10期页码 72-76

摘要：

通过对造纸工业中黑液污染治理的研究，提出了制浆造纸提取黑液的蒸发浓缩+喷雾干燥的新工艺，对已在实践中运用过的蒸发+喷雾干燥工艺加以研究、归纳，并对蒸发+喷雾干燥的新工艺进行了经济分析。实践证实，运用该工艺不仅能实现制浆造纸黑液零污染排放的达标治理，而且可获得木质素类副产品，为企业增强了活力。

关键词：造纸黑液浓缩蒸发喷雾干燥经济分析

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Leaching characteristics of heavy metals during cement stabilization of fly ash from municipal solid waste incinerators

LIANG Shunwen, JIANG Jianguo, ZHANG Yan, XU Xin

《环境科学与工程前沿（英文）》 2008年第2卷第3期页码 358-363 doi: 10.1007/s11783-008-0060-6

摘要： The leaching characteristics of heavy metals in products of cement stabilization of fly ash from a municipal solid waste incinerator were investigated in this paper. The stabilization of heavy metals such as Cd, Pb, Cu, and Zn in fly ash from such incinerators was examined through the national standard method in China based on the following factors: additive quantity of cement and NaS, curing time, and pH of leaching liquor. The results showed that as more additives were used, less heavy metals were leached except for Pb, which is sensitive to pH of the leachate, and the worse effect was observed for Cd. The mass ratio of cement to fly ash = 10% is the most appropriate parameter according to the national standard method. When the hydration of cement was basically finished, stabilization of heavy metals did not vary after curing for 1 d. The mixtures of cement and fly ash had excellent adaptability to environmental pH. The pH of leachate was maintained at 7 when pH of leaching liquor varied from 3 to 11.

关键词： heavy national standard environmental leachate liquor

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Novel coprecipitation–oxidation method for recovering iron from steel waste pickling liquor

Shejiang Liu, Hongyang Yang, Yongkui Yang, Yupeng Guo, Yun Qi

《环境科学与工程前沿（英文）》 2017年第11卷第1期 doi: 10.1007/s11783-017-0902-1

摘要： Coprecipitation–oxidation method was developed to recover the iron from wastewater. Fe O nanoparticles were well synthesized from steel waste pickling liquor. Promoters greatly improved the properties of synthesized Fe O nanoparticle. Real-time control of the Fe /Fe molar ratio was achieved by ORP monitoring. Waste pickling liquors (WPLs) containing high concentrations of iron and acid are hazardous waste products from the steel pickling processes. A novel combined coprecipitation–oxidation method for iron recovery by Fe O nanoparticle production from the WPLs was developed in this study. An oxidation–reduction potential monitoring method was developed for real-time control of the Fe /Fe molar ratio. The key coprecipitation–oxidation parameters were determined using the orthogonal experimental design method. The use of promoters greatly improved the Fe O nanoparticle crystallinity, size, magnetization, and dispersion. X-ray diffraction patterns showed that the produced Fe O nanoparticles were single phase. The Fe O nanoparticles were approximately spherical and slightly agglomerated. Vibrating sample magnetometry showed that the Fe O nanoparticles produced from the WPLs had good magnetic properties, with a saturation magnetization of 80.206 emu·g and a remanence of 10.500 emu·g . The results show that this novel coprecipitation–oxidation method has great potential for recycling iron in WPLs.

关键词： Waste pickling liquor Coprecipitation–oxidation Fe₃O₄ nanoparticles Oxidation–reduction potential Promoter

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humic acid and metal ions on the debromination of BDE209 by nZVM prepared from steel pickling waste liquor

Yuling CAI,Bin LIANG,Zhanqiang FANG,Yingying XIE,Eric Pokeung TSANG

《环境科学与工程前沿（英文）》 2015年第9卷第5期页码 879-887 doi: 10.1007/s11783-014-0764-8

摘要： As a promising in situ remediation technology, nanoscale zero-valent iron (nZVI) can remove polybrominated diphenyl ethers such as decabromodiphenyl ether (BDE209) effectively, However its use is limited by its high production cost. Using steel pickling waste liquor as a raw material to prepare nanoscale zero-valent metal (nZVM) can overcome this deficiency. It has been shown that humic acid and metal ions have the greatest influence on remediation. The results showed that nZVM and nZVI both can effectively remove BDE209 with little difference in their removal efficiencies, and humic acid inhibited the removal efficiency, whereas metal ions promoted it. The promoting effects followed the order Ni >Cu >Co and the cumulative effect of the two factors was a combination of the promoting and inhibitory individual effects. The major difference between nZVM and nZVI lies in their crystal form, as nZVI was found to be amorphous while that of nZVM was crystal. However, it was found that both nZVM and nZVI removed BDE209 with similar removal efficiencies. The effects and cumulative effects of humic acid and metal ions on nZVM and nZVI were very similar in terms of the efficiency of the BDE209 removal.

关键词： steel pickling waste liquor nanoscale zero-valet metal nanoscale zero-valent iron humic acid metal ion