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Synthesis and characterization of 2,5-bis[4-(2-arylvinyl)phenyl]-1,3,4-oxadiazoles with two-photon fluorescence properties

ZHU Xiaoqin, QIAN Ying, LU Zhifeng

《化学科学与工程前沿（英文）》 2007年 第1卷 第4期   页码 381-384 doi: 10.1007/s11705-007-0069-6

摘要： Four novel 2,5-bis[4-(2-arylvinyl)phenyl]-1,3,4-oxadiazoles that exhibit strong two-photon absorption and enhanced two-photon excited fluorescence were designed and synthesized based on push-core-pull-core-push molecules built from embedding electron-transporting 1,3,4-oxadiazole in aromatic conjugated system through Wittig-Horner reaction. Their chemical structures were determined to show trans-vinylene character according to infrared (IR) and H nuclear magnetic resonance (NMR) spectra. A very effective energy transfer from the excited units to the ?-conjugated bridging unit can enhance the two-photon absorption and two-photon fluorescence.

关键词： 2-arylvinyl     trans-vinylene character     effective     fluorescence     push-core-pull-core-push    

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带多局部约束的改进push-sum框架分布式优化及其在智能电网中的应用

徐谦,俞楚天,袁翔,韦梦立,刘洪喆

《信息与电子工程前沿（英文）》 2023年 第24卷 第9期   页码 1253-1260 doi: 10.1631/FITEE.2200596

摘要： 为此，在改进的push-sum框架下，本文设计了新的分布式优化算法，并在强连通图的假设下给出了其严格的收敛分析。最后，仿真结果证明了所提算法的良好性能。

关键词： 分布式优化     非一致约束     改进push-sum框架    

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全球计时器暂停闰秒计时

Chris Palmer

《工程（英文）》 2023年 第27卷 第8期   页码 6-7 doi: 10.1016/j.eng.2023.06.003

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先进天线赋能无线互联

陆贵文, 段宝岩

《工程（英文）》 2022年 第11卷 第4期   页码 1-2 doi: 10.1016/j.eng.2022.03.003

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Postprocessor development for ultrasonic cutting of honeycomb core curved surface with a straight blade

《机械工程前沿（英文）》 2023年 第18卷 第1期 doi: 10.1007/s11465-022-0729-8

摘要： When ultrasonically cutting honeycomb core curved parts, the tool face of the straight blade must be along the curved surface’s tangent direction at all times to ensure high-quality machining of the curved surface. However, given that the straight blade is a nonstandard tool, the existing computer-aided manufacturing technology cannot directly realize the above action requirement. To solve this problem, this paper proposed an algorithm for extracting a straight blade real-time tool face vector from a 5-axis milling automatically programmed tool location file, which can realize the tool location point and tool axis vector conversion from the flat end mill to the straight blade. At the same time, for the multi-solution problem of the rotation axis, the dependent axis rotation minimization algorithm was introduced, and the spindle rotation algorithm was proposed for the tool edge orientation problem when the straight blade is used to machine the curved part. Finally, on the basis of the MATLAB platform, the dependent axis rotation minimization algorithm and spindle rotation algorithm were integrated and compiled, and the straight blade ultrasonic cutting honeycomb core postprocessor was then developed. The model of the machine tool and the definition of the straight blade were conducted in the VERICUT simulation software, and the simulation machining of the equivalent entity of the honeycomb core can then be realized. The correctness of the numerical control program generated by the postprocessor was verified by machining and accuracy testing of the two designed features. Observation and analysis of the simulation and experiment indicate that the tool pose is the same under each working condition, and the workpieces obtained by machining also meet the corresponding accuracy requirements. Therefore, the postprocessor developed in this paper can be well adapted to the honeycomb core ultrasonic cutting machine tool and realize high-quality and high-efficient machining of honeycomb core composites.

关键词： honeycomb core     straight blade     ultrasonic cutting     tool pose     postprocessor    

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基于适用概率匹配与多维情境驱动的设计知识推送技术 None

Shu-you ZHANG, Ye GU, Xiao-jian LIU, Jian-rong TAN

《信息与电子工程前沿（英文）》 2018年 第19卷 第2期   页码 235-245 doi: 10.1631/FITEE.1700763

摘要： 为了提高产品智能设计过程中设计知识的使用效率和质量，有必要向设计人员主动推送设计知识。知识推送主要包括知识匹配和匹配结果的合理推送两个方面。针对现有知识匹配通常缺乏智能性和匹配结果推送缺少个性化的问题，提出基于适用概率匹配和多维情境驱动的设计知识推送技术。构建包括设计知识表示向量、设计案例特征向量和映射布尔矩阵等的训练样本集，通过贝叶斯理论计算设计知识适用与不适用于设计内容的概率，即二者之间的匹配度，得到推送知识集。构建等级化设计内容模型对推送知识集进行过滤，通过设计知识、设计上下文、设计内容和设计人员等多维情境驱动，实现个性化的设计知识推送。在数控机床智能设计平台中的知识推送应用，证明了该技术的可行性和正确性。

关键词： 产品设计；知识推送；适用概率匹配；多维情境；个性化    

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Establishment and verification of a shrinking core model for dilute acid hydrolysis of lignocellulose

Cunwen WANG, Xiaoling DUAN, Weiguo WANG, Zihao LI, Yuanhang QIN

《能源前沿（英文）》 2012年 第6卷 第4期   页码 413-419 doi: 10.1007/s11708-012-0212-z

摘要： The kinetics of lignocellulose hydrolysis under the conditions of high temperature and dilute acid (mass fraction 0.05%) was investigated in this paper. By studying the reducing sugar concentration versus reaction temperature (170°C–220°C) and reaction time (150–1800 s) during the hydrolysis process of five kinds of crop straw (rice, wheat, cotton, rape and corn), the shrinking core model was established, and the differential equation of the model and its analytical solution were obtained. With a numerical calculation method, the kinetic equation was estimated, and the degradation of reducing sugar obeyed first-order kinetics was obtained. The calculated results from the equations agreed well with the original experimental data. The calculation by the model showed that the reducing sugar concentration increases as the size of the particles decrease, and the uniform particles increase.

关键词： lignocellulose     dilute acid hydrolysis     shrinking core model    

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Push recovery for the standing under-actuated bipedal robot using the hip strategy

Chao LI,Rong XIONG,Qiu-guo ZHU,Jun WU,Ya-liang WANG,Yi-ming HUANG

《信息与电子工程前沿（英文）》 2015年 第16卷 第7期   页码 579-593 doi: 10.1631/FITEE.14a0230

摘要： This paper presents a control algorithm for push recovery, which particularly focuses on the hip strategy when an external disturbance is applied on the body of a standing under-actuated biped. By analyzing a simplified dynamic model of a bipedal robot in the stance phase, it is found that horizontal stability can be maintained with a suitably controlled torque applied at the hip. However, errors in the angle or angular velocity of body posture may appear, due to the dynamic coupling of the translational and rotational motions. To solve this problem, different hip strategies are discussed for two cases when (1) external disturbance is applied on the center of mass (CoM) and (2) external torque is acting around the CoM, and a universal hip strategy is derived for most disturbances. Moreover, three torque primitives for the hip, depending on the type of disturbance, are designed to achieve translational and rotational balance recovery simultaneously. Compared with closed-loop control, the advantage of the open-loop methods of torque primitives lies in rapid response and reasonable performance. Finally, simulation studies of the push recovery of a bipedal robot are presented to demonstrate the effectiveness of the proposed methods.

关键词： Push recovery     Balance control     Bipedal robot     Hip strategy    

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Recent advances in gold-metal oxide core-shell nanoparticles: Synthesis, characterization, and their

Michelle Lukosi,Huiyuan Zhu,Sheng Dai

《化学科学与工程前沿（英文）》 2016年 第10卷 第1期   页码 39-56 doi: 10.1007/s11705-015-1551-1

摘要： Heterogeneous catalysis with core-shell structures has been a large area of focus for many years. This paper reviews the most recent work and research in core-shell catalysts utilizing noble metals, specifically gold, as the core within a metal oxide shell. The advantage of the core-shell structure lies in its capacity to retain catalytic activity under thermal and mechanical stress, which is a pivotal consideration when synthesizing any catalyst. This framework is particularly useful for gold nanoparticles in protecting them from sintering so that they retain their size, structure, and most importantly their catalytic efficiency. The different methods of synthesizing such a structure have been compiled into three categories: seed-mediated growth, post selective oxidation treatment, and one-pot chemical synthesis. The selective oxidation of carbon monoxide and reduction of nitrogen containing compounds, such as nitrophenol and nitrostyrene, have been studied over the past few years to evaluate the functionality and stability of the core-shell catalysts. Different factors that could influence the catalyst’s performance are the size, structure, choice of metal oxide shell and noble metal core and thereby the interfacial synergy and lattice mismatch between the core and shell. In addition, the morphology of the shell also plays a critical role, including its porosity, density, and thickness. This review covers the synthesis and characterization of gold-metal oxide core-shell structures, as well as how they are utilized as catalysts for carbon monoxide (CO) oxidation and selective reduction of nitrogen-containing compounds.

关键词： core-shell     characterization     core-shell structure     Different     stability    

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Property-performance relationship of core-shell structured black TiO photocatalyst for environmental

《环境科学与工程前沿（英文）》 2023年 第17卷 第9期 doi: 10.1007/s11783-023-1711-3

摘要：

● Properties and performance relationship of CSBT photocatalyst were investigated.

关键词： Black TiO2     Core-shell structure     Property-performance relationship     Agro-industrial effluent     Environmental remediation    

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Experiment and calculation on seismic behavior of RC composite core walls with concealed steel truss

Wanlin CAO , Weihua CHANG , Changjun ZHAO , Jianwei ZHANG ,

《结构与土木工程前沿（英文）》 2009年 第3卷 第3期   页码 255-261 doi: 10.1007/s11709-009-0043-0

摘要： To improve the seismic performance of reinforced concrete core walls, reinforced concrete composite core walls with concealed steel truss were proposed and systemically investigated. Two 1/6 scale core wall specimens, including a normal reinforced concrete core wall and a reinforced concrete composite core wall with concealed steel truss, were designed. The experimental study on seismic performance under cyclic loading was carried out. The load-carrying capacity, stiffness, ductility, hysteretic behavior and energy dissipation of the core walls were discussed. The test results showed that the seismic performance of core walls is improved greatly by the concealed steel truss. The calculated results were found to agree well with the actual measured ones.

关键词： reinforced concrete     steel truss     core walls     seismic performance    

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Effects of inclination angles of disc cutter on machining quality of Nomex honeycomb core in ultrasonic

Yidan WANG, Renke KANG, Yan QIN, Qian MENG, Zhigang DONG

《机械工程前沿（英文）》 2021年 第16卷 第2期   页码 285-297 doi: 10.1007/s11465-021-0631-9

摘要： Ultrasonic cutting with a disc cutter is an advanced machining method for the high-quality processing of Nomex honeycomb core. The machining quality is influenced by ultrasonic cutting parameters, as well as tool orientations, which are determined by the multi-axis machining requirements and the angle control of the cutting system. However, in existing research, the effect of the disc cutter orientation on the machining quality has not been studied in depth, and practical guidance for the use of disc cutters is lacking. In this work, the inclined ultrasonic cutting process with a disc cutter was analyzed, and cutting experiments with different inclination angles were conducted. The theoretical residual height models of the honeycomb core, as a result of the lead and tilt angles, were established and verified with the results obtained by a linear laser displacement sensor. Research shows that the residual height of the honeycomb core, as a result of the tilt angle, is much larger than that as a result of the lead angle. Furthermore, the tearing of the cell wall on the machined surface was observed, and the effects of the ultrasonic vibration, lead angle, and tilt angle on the tear rate and tear length of the cell wall were studied. Experimental results revealed that ultrasonic vibration can effectively decrease the tearing of the cell wall and improve the machining quality. Changes in the tilt angle have less effect than changes in the lead angle on the tearing of the cell wall. The determination of inclination angles should consider the actual processing requirements for the residual height and the machining quality of the cell wall. This study investigates the influence of the inclination angles of a disc cutter on the machining quality of Nomex honeycomb core in ultrasonic cutting and provides guidelines for machining.

关键词： Nomex honeycomb core     disc cutter     inclined ultrasonic cutting     machining quality    

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Improving performance portability for GPU-specific OpenCL kernels onmulti-core/many-coreCPUs by analysis-based

Mei WEN,Da-fei HUANG,Chang-qing XUN,Dong CHEN

《信息与电子工程前沿（英文）》 2015年 第16卷 第11期   页码 899-916 doi: 10.1631/FITEE.1500032

摘要： OpenCL is an open heterogeneous programming framework. Although OpenCL programs are functionally portable, they do not provide performance portability, so code transformation often plays an irreplaceable role. When adapting GPU-specific OpenCL kernels to run on multi-core/many-core CPUs, coarsening the thread granularity is necessary and thus has been extensively used. However, locality concerns exposed in GPU-specific OpenCL code are usually inherited without analysis, which may give side-effects on the CPU performance. Typically, the use of OpenCL’s local memory on multi-core/many-core CPUs may lead to an opposite performance effect, because local-memory arrays no longer match well with the hardware and the associated synchronizations are costly. To solve this dilemma, we actively analyze the memory access patterns using array-access descriptors derived from GPU-specific kernels, which can thus be adapted for CPUs by (1) removing all the unwanted local-memory arrays together with the obsolete barrier statements and (2) optimizing the coalesced kernel code with vectorization and locality re-exploitation. Moreover, we have developed an automated tool chain that makes this transformation of GPU-specific OpenCL kernels into a CPU-friendly form, which is accompanied with a scheduler that forms a new OpenCL runtime. Experiments show that the automated transformation can improve OpenCL kernel performance on a multi-core CPU by an average factor of 3.24. Satisfactory performance improvements are also achieved on Intel’s many-integrated-core coprocessor. The resultant performance on both architectures is better than or comparable with the corresponding OpenMP performance.

关键词： OpenCL     Performance portability     Multi-core/many-core CPU     Analysis-based transformation    

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Interfacial charge transfer and photocatalytic activity in a reverse designed BiO/TiO core-shell

《能源前沿（英文）》 2021年 第15卷 第3期   页码 732-743 doi: 10.1007/s11708-021-0772-x

摘要： In this study, the electronic and photocatalytic properties of core-shell heterojunctions photocatalysts with reversible configuration of TiO2 and Bi2O3 layers were studied. The core-shell nanostructure, obtained by efficient control of the sol-gel polymerization and impregnation method of variable precursors of semiconductors, makes it possible to study selectively the role of the interfacial charge transfer in each configuration. The morphological, optical, and chemical composition of the core-shell nanostructures were characterized by high-resolution transmission electron microscopy, UV-visible spectroscopy and X-ray photoelectron spectroscopy. The results show the formation of homogenous TiO2 anatase and Bi2O3 layers with a thickness of around 10 and 8 nm, respectively. The interfacial charge carrier dynamic was tracked using time resolved microwave conductivity and transition photocurrent density. The charge transfer, their density, and lifetime were found to rely on the layout layers in the core-shell nanostructure. In optimal core-shell design, Bi2O3 collects holes from TiO2, leaving electrons free to react and increase by 5 times the photocatalytic efficiency toward H2 generation. This study provides new insight into the importance of the design and elaboration of optimal heterojunction based on the photocatalyst system to improve the photocatalytic activity.

关键词： photocatalysis     core-shell     heterojunction     H2     TiO2     Bi2O3    

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Construction of PS/PNIPAM core-shell particles and hollow spheres by using hydrophobic interaction and

ZHU Dongmei, WANG Fei, GAO Cuiling, XU Zheng

《化学科学与工程前沿（英文）》 2008年 第2卷 第3期   页码 253-256 doi: 10.1007/s11705-008-0049-5

摘要： This paper reports an easy and effective way to fabricate polystyrene/poly (-isopropylacrylamide) (PS/PNIPAM) core-shell particles and PNIPAM hollow spheres. The main point of the method is to take advantage of the hydrophobic interaction between initiator and PS particles. The hydrophobic azodiisobutyronitriles automatically concentrate around the PS particles and initiate polymerization of -isopropylacrylamide (NIPAM) and the crosslinker methylene bisacrylamide (MBA), which dissolve in the aqueous phase, at the surface of the PS nanoparticles. Then, PNIPAM adheres to the PS particles to form a core-shell structure as a result of their hydrophobic interaction. This interaction is due to the unique property of PNIPAM, namely, its ability to transition from hydrophilic to hydrophobic when the temperature rises to 32°C. Furthermore, the hollow PNIPAM spheres were obtained by etching the PS core with chloroform.

关键词： initiator     core-shell     transition     polystyrene/poly     advantage    

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标题 作者 时间 类型 操作

Synthesis and characterization of 2,5-bis[4-(2-arylvinyl)phenyl]-1,3,4-oxadiazoles with two-photon fluorescence properties

ZHU Xiaoqin, QIAN Ying, LU Zhifeng

期刊论文

带多局部约束的改进push-sum框架分布式优化及其在智能电网中的应用

徐谦,俞楚天,袁翔,韦梦立,刘洪喆

期刊论文

全球计时器暂停闰秒计时

Chris Palmer

期刊论文

先进天线赋能无线互联

陆贵文, 段宝岩

期刊论文

Postprocessor development for ultrasonic cutting of honeycomb core curved surface with a straight blade

期刊论文

基于适用概率匹配与多维情境驱动的设计知识推送技术

Shu-you ZHANG, Ye GU, Xiao-jian LIU, Jian-rong TAN

期刊论文

Establishment and verification of a shrinking core model for dilute acid hydrolysis of lignocellulose

Cunwen WANG, Xiaoling DUAN, Weiguo WANG, Zihao LI, Yuanhang QIN

期刊论文

Push recovery for the standing under-actuated bipedal robot using the hip strategy

Chao LI,Rong XIONG,Qiu-guo ZHU,Jun WU,Ya-liang WANG,Yi-ming HUANG

期刊论文

Recent advances in gold-metal oxide core-shell nanoparticles: Synthesis, characterization, and their

Michelle Lukosi,Huiyuan Zhu,Sheng Dai

期刊论文

Property-performance relationship of core-shell structured black TiO photocatalyst for environmental

期刊论文

Experiment and calculation on seismic behavior of RC composite core walls with concealed steel truss

Wanlin CAO , Weihua CHANG , Changjun ZHAO , Jianwei ZHANG ,

期刊论文

Effects of inclination angles of disc cutter on machining quality of Nomex honeycomb core in ultrasonic

Yidan WANG, Renke KANG, Yan QIN, Qian MENG, Zhigang DONG

期刊论文

Improving performance portability for GPU-specific OpenCL kernels onmulti-core/many-coreCPUs by analysis-based

Mei WEN,Da-fei HUANG,Chang-qing XUN,Dong CHEN

期刊论文

Interfacial charge transfer and photocatalytic activity in a reverse designed BiO/TiO core-shell

期刊论文

Construction of PS/PNIPAM core-shell particles and hollow spheres by using hydrophobic interaction and

ZHU Dongmei, WANG Fei, GAO Cuiling, XU Zheng

期刊论文