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Anticorrosive composite self-healing coating enabled by solar irradiation

《化学科学与工程前沿（英文）》 2022年第16卷第9期页码 1355-1366 doi: 10.1007/s11705-022-2147-1

摘要： Self-healing coatings for long-term corrosion protection have received much interest in recent years. However, most self-healing coatings rely on healants released from microcapsules, dynamic bonds, shape memory, or thermoplastic materials, which generally suffer from limited healing times or harsh conditions for self-healing, such as high temperature and UV radiation. Herein, we present a composite coating with a self-healing function under easily accessible sunlight by adding Fe₃O₄ nanoparticles and tetradecanol into epoxy resin. Tetradecanol, with its moderate melting point, and Fe₃O₄ nanoparticles serve as a phase-change component and photothermal material in an epoxy coating system, respectively. Fe₃O₄ nanoparticles endow this composite self-healing coating with good photothermal properties and a rapid thermal response time under simulated solar irradiation as well as outdoor real sunlight. Tetradecanol can flow to and fill defects by phase transition at low temperatures. Therefore, artificial defects created in this type of self-healing coating can be healed by the liquified tetradecanol induced by the photothermal effect of Fe₃O₄ nanoparticles under simulated solar irradiation. The healed coating can still serve as a good barrier for the protection of the underlying carbon steel. These excellent properties make this self-healing coating an excellent candidate for various engineering applications.

关键词： self-healing coating phase transition photothermal effect corrosion protection

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Elastic modulus and thermal stress in coating during heat cycling with different substrate shapes

Daniel GAONA,Alfredo VALAREZO

《机械工程前沿（英文）》 2015年第10卷第3期页码 294-300 doi: 10.1007/s11465-015-0351-0

摘要：

The elastic modulus of a deposit (E_d) can be obtained by monitoring the temperature (?T) and curvature (?k) of a one-side coated long plate, namely, a one-dimensional (1D) deformation model. The aim of this research is to design an experimental setup that proves whether a 1D deformation model can be scaled for complex geometries. The setup includes a laser displacement sensor mounted on a robotic arm capable of scanning a specimen surface and measuring its deformation. The reproducibility of the results is verified by comparing the present results with Stony Brook University Laboratory’s results. The ?k-?T slope error is less than 8%, and the E_d estimation error is close to 2%. These values reveal the repeatability of the experiments. Several samples fabricated with aluminum as the substrate and 100MXC nanowire (Fe and Cr alloy) as the deposit are analyzed and compared with those in finite element (FE) simulations. The linear elastic behavior of 1D (flat long plate) and 2D (squared plate) specimens during heating/cooling cycles is demonstrated by the high linearity of all ?k-?T curves (over 97%). The E_d values are approximately equal for 1D and 2D analyses, with a median of 96 GPa and standard deviation of 2 GPa. The correspondence between the experimental and simulated results for the 1D and 2D specimens reveals that deformation and thermal stress in coated specimens can be predicted regardless of specimen geometry through FE modeling and by using the experimental value of E_d. An example of a turbine-blade-shaped substrate is presented to validate the approach.

关键词： in-plane Young’s modulus curvature temperature thermal stress coating

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The feasibility of coating by cooling crystallization on ibuprofen naked tablets

Fatima Mameri, Ouahiba Koutchoukali, Mohamed Bouhelassa, Anne Hartwig, Leila Nemdili, Joachim Ulrich

《化学科学与工程前沿（英文）》 2017年第11卷第2期页码 211-219 doi: 10.1007/s11705-017-1619-1

摘要： Sugar spray coating is a frequently used process in the pharmaceutical industry. However, this process presents the disadvantage to form an amorphous coating around the active ingredient. A crystalline coating formed on the surface of a tablet is highly desirable. Recently, a new process of coating by cooling crystallization has been developed and applied on bisacodyl pastilles obtained by melt crystallization. In this work, we investigated the feasibility of coating by cooling crystallization on ibuprofen “naked tablets” manufactured by compression. In the first part of this work, the solubility and the metastable zone width have been determined experimentally for the coating solution because they are essential factors for any crystallization process. In the second part, the coating process is investigated on the operating conditions that affect the surface morphology and the crystal growth rate. These experimental conditions include concentration of the coating solution, degree of sub-cooling, agitation speed, retention time, and surface properties of the naked ibuprofen tablets. The results show that naked tablet coating by cooling crystallization is feasible and can be applied in the pharmaceutical industry.

关键词： coating solution crystallization ibuprofen tablets sucrose

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Erratum to: Enhancing the photoelectrochemical performance of p-silicon through TiO coating decorated

《能源前沿（英文）》 2022年第16卷第5期页码 876-877 doi: 10.1007/s11708-022-0832-x

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A novel composite coating mesh film for oil-water separation

Futao QIN, Zhijia YU, Xinhui FANG, Xinghua LIU, Xiangyu SUN

《化学科学与工程前沿（英文）》 2009年第3卷第1期页码 112-118 doi: 10.1007/s11705-009-0149-x

摘要： Polytetrafluoroethylene-polyphenylene sulfide composite coating mesh film was successfully prepared by a simple layered transitional spray-plasticizing method on a stainless steel mesh. It shows super-hydrophobic and super-oleophilic properties. The contact angle of this mesh film is 156.3° for water, and close to 0° for diesel oil and kerosene. The contact angle hysteresis of water on the mesh film is 4.3°. The adhesive force between the film and substrate is grade 0, the flexibility is 1 mm and the pencil hardness is 4H. An oil-water separation test was carried out for oil-contaminated water in a six-stage super-hydrophobic film separator. The oil removal rate can reach about 99%.

关键词： super-hydrophobic super-oleophilic composite coating mesh film separation of oil and water

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Accumulated damage process of thermal sprayed coating under rolling contact by acoustic emission technique

Jia XU,Zhen-yu ZHOU,Zhong-yu PIAO

《机械工程前沿（英文）》 2016年第11卷第3期页码 227-232 doi: 10.1007/s11465-016-0395-9

摘要：

The accumulated damage process of rolling contact fatigue (RCF) of plasma-sprayed coatings was investigated. The influences of surface roughness, loading condition, and stress cycle frequency on the accumulated damage status of the coatings were discussed. A ball-on-disc machine was employed to conduct RCF experiments. Acoustic emission (AE) technique was introduced to monitor the RCF process of the coatings. AE signal characteristics were investigated to reveal the accumulated damage process. Result showed that the polished coating would resist the asperity contact and remit accumulated damage. The RCF lifetime would then extend. Heavy load would aggravate the accumulated damage status and induce surface fracture. Wear became the main failure mode that reduced the RCF lifetime. Frequent stress cycle would aggravate the accumulated damage status and induce interface fracture. Fatigue then became the main failure mode that also reduced the RCF lifetime.

关键词： accumulated damage spray coating rolling contact fatigue acoustic emission

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Enhancing the photoelectrochemical performance of p-silicon through TiO coating decorated with mesoporous

《能源前沿（英文）》 2021年第15卷第3期页码 772-780 doi: 10.1007/s11708-021-0783-7

摘要： MoS₂ is a promising electrocatalyst for hydrogen evolution reaction and a good candidate for cocatalyst to enhance the photoelectrochemical (PEC) performance of Si-based photoelectrode in aqueous electrolytes. The main challenge lies in the optimization of the microstructure of MoS₂, to improve its catalytic activity and to construct a mechanically and chemically stable cocatalyst/Si photocathode. In this paper, a highly-ordered mesoporous MoS₂ was synthesized and decorated onto a TiO₂ protected p-silicon substrate. An additional TiO₂ necking was introduced to strengthen the bonding between the MoS₂ particles and the TiO₂ layer. This meso-MoS₂/TiO₂/p-Si hybrid photocathode exhibited significantly enhanced PEC performance, where an onset potential of +0.06 V (versus RHE) and a current density of −1.8 mA/cm² at 0 V (versus RHE) with a Faradaic efficiency close to 100% was achieved in 0.5 mol/L H₂SO₄. Additionally, this meso-MoS₂/TiO₂/p-Si photocathode showed an excellent PEC ability and durability in alkaline media. This paper provides a promising strategy to enhance and protect the photocathode through high-performance surface cocatalysts.

关键词： photoelectrocatalysis hydrogen evolution Si photocathode mesoporous MoS₂

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Preparation of solar selective absorbing CuO coating for medium temperature application

HUANG Qunwu, WANG Yiping, LI Jinhua

《化学科学与工程前沿（英文）》 2007年第1卷第3期页码 256-260 doi: 10.1007/s11705-007-0046-0

摘要： A new method of preparing CuO solar selective absorbing coating for medium temperature is presented. After pretreatment, brass was overlaid with CuO by chemical plating. The effects of reactant concentration, reaction temperature and reaction time on the absorptivity of CuO coating were investigated. The optimized condition of preparing CuO coating was obtained. The CuO coating was analyzed with X-ray photoelectron spectroscopy (XPS) and scanning electron microscopy (SEM). In order to prolong the period of use, the CuO coating was protected by TiO. The experiment shows that the TiO/CuO coating is more heat-resistant, acid-resistant, and wear resistant than CuO coating, without losing absorptivity markedly. The TiO coating can reduce emissivity and protect the CuO coating.

关键词： photoelectron spectroscopy temperature pretreatment absorptivity microscopy

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DOW CORNING 1-2577 Conformal Coating as an efficient diffusion material for cathode in the microbial

Yanping HOU, Haiping LUO, Guangli LIU, Renduo ZHANG, Yong LUO, Bangyu QIN, Shanshan CHEN

《环境科学与工程前沿（英文）》 2013年第7卷第4期页码 526-530 doi: 10.1007/s11783-013-0532-1

摘要： In this study, DOW CORNING 1-2577 Conformal Coating was proposed for the cathode diffusion layer of the microbial fuel cell (MFC). In MFCs, stainless steel mesh cathodes using DOW CORNING 1-2577 Conformal Coating/carbon as the diffusion layer and two poly (dimethylsiloxane) (PDMS)/carbon diffusion layers and carbon cloth cathode with four poly (tetrafluoroethylene) (PTFE) diffusion layers were constructed for comparison. Under the same operational condition, the MFCs with the DOW CORNING 1-2577 Conformal Coating/carbon diffusion layer produced the maximum power density of 1585±52 mW·m , compared with those using poly (tetrafluoroethylene) (PTFE) diffusion layers (1421±45 mW·m ) and poly (dimethylsiloxane) (PDMS)/carbon diffusion layers (1353±49 mW·m ). The DOW CORNING 1-2577 Conformal Coating could be an alternative for the diffusion layer construction in the MFC due to its remarkable performance and much simple construction procedure.

关键词： microbial fuel cell diffusion layer power density DOW CORNING1-2577 Conformal Coating

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Residual stresses in coating-based systems, part I: Mechanisms and analytical modeling

ZHANG Xiancheng, WU Yixiong, XU Binshi, WANG Haidou

《机械工程前沿（英文）》 2007年第2卷第1期页码 1-12 doi: 10.1007/s11465-007-0001-2

摘要： Thin films and multi-layered coatings comprised of different classes of materials are often used for various functional devices. The thermo-mechanical integrity of these systems is becoming a major concern and is strongly related to the residual stresses because of the fabrication processes. In this paper, the sources of the residual stresses in the coating-based systems and the concept of misfit strain were briefly reviewed. Analytical models were developed to predict the residual stresses in multi-layered film structures or coating-based systems using the force and moment balances. In addition, the residual stress distributions in the func tionally and compositionally graded coatings were also analyzed.

关键词： briefly different thermo-mechanical integrity addition residual

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Residual stresses in coating-based systems, part II: Optimal designing methodologies

ZHANG Xiancheng, WU Yixiong, XU Binshi, WANG Haidou

《机械工程前沿（英文）》 2007年第2卷第2期页码 125-136 doi: 10.1007/s11465-007-0022-x

摘要： In this part of the work, different cases are studied to illustrate the implementation of the analytical models that have been developed in Part I [Front. Mech. Eng. China, 2007, 2(1): 1 12]. Different topics are involved in the optimal design of coating-based systems. Some essential relations among material properties and dimensions of the coating and substrate and the residual stress variations are reflected. For the multilayered coating-based systems, some optimal design methodologies are proposed, such as the decrease in stress discontinuity at the interface between the adjacent layers, the curvature as a function of the coating thickness, the effect of the interlayer on the residual stress redistribution, and so on. For the single-layered coating-based systems, some typical approximations that are often used to predict the residual stresses in the coating-based system or bilayer structure are corrected. A simplified model for predicting the quenching stress in a coating is also developed.

关键词： function different substrate interlayer implementation

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激光熔覆NiCrAl-陶瓷涂层的显微组织研究

陈庆华,魏仑,龙晋明,李俊昌

《中国工程科学》 2001年第3卷第10期页码 64-71

摘要：

运用激光熔覆技术在40Cr钢表面制备了(TiO₂+B₂O₃+Al₂O₃+TiB₂)/NiCrAl金属陶瓷涂层，其中的TiB₂和Al₂O₃陶瓷颗粒在激光加工过程中原位反应生成；对熔覆层的组织、物相、元素分布和显微硬度分布特征进行了分析研究；熔覆层中的主相依次分别是γ-Ni,γ′,Al₂O₃和TiB₂，熔覆层的微观结构和硬度主要和激光处理参数和熔覆层化学组成有关^［1～9］；陶瓷相的原位生成和加入，大大改善了熔覆层的硬度和覆层/基体界面的结合性能。

关键词：激光熔覆金属陶瓷微观组织物相显微硬度

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Development of a new wear resistant coating by arc spraying of a steel-based cored wire

Lidong ZHAO, Pia KUTSCHMANN, Binyou FU, Dingyong HE

《机械工程前沿（英文）》 2009年第4卷第1期页码 1-4 doi: 10.1007/s11465-009-0012-2

摘要： In the present study, a cored wire of 304 L stainless steel as sheath material and NiB and WC-12Co as filler materials was designed and deposited to produce a new wear resistant coating containing amorphous phase by arc spraying. The microstructure of the coating was investigated. The porosity and hardness of the coating were determined. The wear performance of the coating was evaluated. The XRD and TEM analyses showed that there are high volume of amorphous phase and very fine crystalline grains in the coating. DTA measurements revealed that the crystallization of the amorphous phase occurred at 579.2°C. Because metallurgical processes for single droplets were non-homogenous during spraying, the lamellae in the coating have different hardness values, which lie between about 700 and 1250 HV . The abrasive wear test showed that the new Fe-based coating was very wear resistant.

关键词： amorphous phase arc spraying microstructure wear cored wire

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基于同步波动原理的抗冲蚀弹性涂层设计

郭源君,肖华林,徐大清,李文斌

《中国工程科学》 2008年第10卷第9期页码 60-63

摘要：

基于过流面冲蚀波纹形貌特征与流体边界层扰动波参数的对应关系，提出了实现弹性涂层边壁与边界层扰动波的同步波动，从而变边壁被动承受粒子冲击为主动回避与粒子的碰撞的抗冲蚀设计思想；分析了实现弹性涂层边壁与边界层扰动波同步波动的条件，并由此确定出弹性涂层的材料常数。

关键词：冲蚀边界层弹性边壁弹性涂层同步波动

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Progress in terahertz nondestructive testing: A review

Shuncong ZHONG

《机械工程前沿（英文）》 2019年第14卷第3期页码 273-281 doi: 10.1007/s11465-018-0495-9

摘要： Terahertz (THz) waves, whose frequencies range between microwave and infrared, are part of the electromagnetic spectrum. A gap exists in THz literature because investigating THz waves is difficult due to the weak characteristics of the waves and the lack of suitable THz sources and detectors. Recently, THz nondestructive testing (NDT) technology has become an interesting topic. This review outlines several typical THz devices and systems and engineering applications of THz NDT techniques in composite materials, thermal barrier coatings, car paint films, marine protective coatings, and pharmaceutical tablet coatings. THz imaging has higher resolution but lower penetration than ultrasound imaging. This review presents the significance and advantages provided by the emerging THz NDT technique.

关键词： terahertz pulsed imaging (TPI) nondestructive testing (NDT) composite material thermal barrier coating

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标题作者时间类型操作

Anticorrosive composite self-healing coating enabled by solar irradiation

期刊论文

Elastic modulus and thermal stress in coating during heat cycling with different substrate shapes

Daniel GAONA,Alfredo VALAREZO

期刊论文

The feasibility of coating by cooling crystallization on ibuprofen naked tablets

Fatima Mameri, Ouahiba Koutchoukali, Mohamed Bouhelassa, Anne Hartwig, Leila Nemdili, Joachim Ulrich

期刊论文

Erratum to: Enhancing the photoelectrochemical performance of p-silicon through TiO coating decorated

期刊论文

A novel composite coating mesh film for oil-water separation

Futao QIN, Zhijia YU, Xinhui FANG, Xinghua LIU, Xiangyu SUN

期刊论文

Accumulated damage process of thermal sprayed coating under rolling contact by acoustic emission technique

Jia XU,Zhen-yu ZHOU,Zhong-yu PIAO

期刊论文

Enhancing the photoelectrochemical performance of p-silicon through TiO coating decorated with mesoporous

期刊论文

Preparation of solar selective absorbing CuO coating for medium temperature application

HUANG Qunwu, WANG Yiping, LI Jinhua

期刊论文

DOW CORNING 1-2577 Conformal Coating as an efficient diffusion material for cathode in the microbial

Yanping HOU, Haiping LUO, Guangli LIU, Renduo ZHANG, Yong LUO, Bangyu QIN, Shanshan CHEN

期刊论文

Residual stresses in coating-based systems, part I: Mechanisms and analytical modeling

ZHANG Xiancheng, WU Yixiong, XU Binshi, WANG Haidou

期刊论文

Residual stresses in coating-based systems, part II: Optimal designing methodologies

ZHANG Xiancheng, WU Yixiong, XU Binshi, WANG Haidou

期刊论文

激光熔覆NiCrAl-陶瓷涂层的显微组织研究

陈庆华,魏仑,龙晋明,李俊昌

期刊论文

Development of a new wear resistant coating by arc spraying of a steel-based cored wire

Lidong ZHAO, Pia KUTSCHMANN, Binyou FU, Dingyong HE

期刊论文

基于同步波动原理的抗冲蚀弹性涂层设计

郭源君,肖华林,徐大清,李文斌

期刊论文

Progress in terahertz nondestructive testing: A review

Shuncong ZHONG

期刊论文

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